GCMS analysis results, Sample AE04385, Mar 2002

NYC 9/11 Public Portal Document Library Search Compound Report

. Data File C:\MSDCHEM\l\DATA\031902\4385.D Vial: 28 Acq On 20 Mar 2002 12:59 pm Operator: McLean Sample RE-INJ 3/1 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 1-(2-Nitroethenyl)azulene $... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

35.53 3.04 ug/L 939521 Perylene-d12 34.18

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-(2-Nitroethenyl)azulene $$ Azu... 199 C12H9NO2 096995-27-6 40 2 ID-(1,2/4,5)11,2'-Anhydro-l-hydr... 199 C10H17NO3 073111-82-7 38 3 Phenothiazine $$ lOH-Phenothiazi... 199 C12H9NS 000092-84-2 38 4 2-Cyano-5-(4-fluorophenyl)pyrimi... 199 C11H6FN3 000000-00-0 27 Abundance Scan 3578 (35.529 min): 4385.D (-) m/z 199.20 100.00% 199

155 5000 57 99 T T T

0-pr d l daar 741,190, 11- 229 281 35.20 35.40 35.60 35.80 m/z 155.20 55.11% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #113878:1-(2-Nitroethenyl)azutene$$ Azulene, 1-(2-nitroe... 199

5000 PPmmmm 35.20 35.40 35.60 35.80 152 m/z 57.05 47.35%

0***1WIPT T 1'1'111 “' I miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #113694: 1D-(1,2/4,5)1’,2’-Anhydro-1-hydroxymethyl-2-hydro... 109

T T T i ■ • ■ ■ i 35.20 35.40 35.60 35.80 69 m/z 99.10 36.03% 5000 43 28 85 184 114

m/z-> O+r LuL 153 20 40 60 80 100 120 140 160 180 200 220 240 260 280 ■ ■ i ■ i ■ ■ “ i ■" ■ i ■ ■

Abundance #113902: Phenothlazine $$ 10H-Phenothlazlne (CAS) $$ ENT 3... 109 ■ ■ l^1 “ 1111111 35.20 35.40 35.60 35.80 TIFTTW) m/z 55.05 32.64%

167 5000

51 69 99 139 WAW m/z—> 0-. mm —Gmmmm it

20 40 60 80 100 '126' 140 160 180 200 220 240 260 280 ■ • i • • ■ ■ 1 ■ •1 ■ i ■ ■ ■ • i • • ■ ■ i 35.20 35.40 35.60 35.80

1385.D 5080302.M Thu Mar 21 06:38:07 2002 Page 3

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