GCMS results for vial 21, Feb 28 2002

NYC 9/11 Public Portal Document

Library Search Compound Report 4 ♦

Data File : C:\MSDCHEM\l\DATA\022702\02578.D Vial: 21 Acq On : 28 Feb 2002 2:18 am Operator: McLean Sample : GC SCAN 2/4 B Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 1-Octene (CAS) $$ Caprylene... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

30.64 1.11 ug/L 835309 Chrysene-dl2 30.36

Hit# of 5 Tj itative ID MW MolForm CAS# Qual

1 1-Octene ( ) $$ Caprylene $$ n... 112 C8H16 000111-66-0 49 2 2-Octene (CAS) $$ oct-2-ene $$ 0... 112 C8H16 000111-67-1 43 3 Octane, /1,1'-oxybis- 242 C16H340 000629-82-3 43 4 1-But ol, 2-ethyl- 102 C6H140 000097-95-0 43 Abundance Scan 3039 (30.640 min): 02578.D (-) m/z 57.10 100.00% 57 8000

6000 71 112

4000 — 2000 30.40 30.60 30.80 31.00

Tl/Z-> TT-p-r 4 4hp 5 .129143157171185199213 ■, 22.26 20 40 60 80 100 120 140 160 180 200 220 240 260 m/z 112.20 56.12%

Abundance #13725:1-Octene (CAS) $$ Caprylene $$ n-1 -Octene $$ .alph... 1 2 8000

6000

4000 70 4 30.40 30.60 30.80 31.00 56 m/z 71.10 54.07% 2000 42 h ’622117113 L98 • | • i i ‘ | '11111 H '11' I “ ‘ ■ I ■ “ ■ I''111 ‘1 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #13735: 2-Octene (CAS) $$ oct-2-ene $$ OCTENE-2 $$ 2-Octen... 112 8000 MAmmmmm 6000 30.40 30.60 30.80 31.00 m/z 70.10 53.70% 4000 70

m/z-> 2000 42 " i • ■ " i'" 20 40 as. 56

60 ■i“ ■•i ‘ • i■ ■ ■ ■ i■ " • i "•11■ ■1 • i“I■1 80 100 120 140 160 180 200 220 240 260 Abundance 57 #177042: Octane, 1,1’-oxybis- > Ar 2 71 30.40 30.60 30.80 31.00 8000 43 m/z 55.10 44.78%

6000 29 4000

/z—> 2000 L . 112 | 127143 165_________ 224 H ’I . .T. 1 .T-1 . )-1 . . . 1 . . . . | . . . . | . . . . | . 20 40 60 80 100 120 140 160 180 200 220 240 260 1’131 TTMfu 30.40 30.60 30.80 31.00

02578.D 5080202.M Fri Mar 01 09:04:57 2002 Page 3

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