NYC 9/11 Public Portal Document
Library Search Compound Report
. Data File C:\MSDCHEM\l\DATA\030402\0131LB.D Vial: 5
Acq On 4 Mar 2002 1:32 pm Operator: McLean
Sample 1/31 Inst : Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator)
Title : Quantitation For Method 508gcscan
Library : C:\DATABASE\WILEY7N.L
Peak Number 3 2-(bromomethyl)-1,8-dimetho... Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
17.88 0.44 ug/L 185323 Acenaphthene-dl0 18.17
Hit# of 5 Tentative MW MolForm CAS# Qual
1 2- (bromomethyl) -1, 8-dimethoxy-9, .. . 360 C17H13BrO4 107960-83-8 52
2 3-Isopropoxy- 1,1,1,7,7-hexamet... 576 C18H52O7S17 071579-69-6 50
3 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 43
4 Pentasiloxane, dodecamethyl- $$ ... 384 C12H36O4Si5 000141-63-9 40
Abundance Scan 1632 (17.879 min): 0131LB.D (-) m/z 73.10 100.00%
73
281
5000 147
327 . ....... ...A.....
17.60 ilso 18.66 18.20
m/z~>
0+ T— '111'11 —21 .31
50 100 150 200 250 300 350 400 450 500 550
m/z 281.10 51.26%
Abundance #305906:2-(bromomethyl>1,8-dimethoxy-9,10-anthracenedion...
281
5000
152 17.60 17.80 18.00 18.20
362 m/z 147.10 42.73%
237
0+ •I-***PA424141IIA1IIIIIS
• I • • • • I • • • • I • • • • IJ • • • I • •
miz-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #379639: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(tr...
73
■ ■ i • ■'' i
A
’ I*’ ■ ' i ■ *
17.60 17.80 18.00 18.20
5000 m/z 326.90 17.83%
147
43
221
21 377 415 519 551
04 .. TPPTTTTT ■ r ■ I ■ r । 1 । । 1 | ih 1 1 । 1 1 । । J* 11 । । । r ।
miz-> 50 100 150 200 2501 300 350 400 450 500 550
Abundance #322218: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trim...
73 147
17'60 17'80 18.00 18.20
m/z 282.10 12.25%
281
5000
369
271 207 940 . 338 [ ____________ _
m/z—>
0- - 117
ntfi 177,4348
r, ।. • . . । . r. . ! . 1. . । 1 । > > ।> । 1 1 ।< ।
50 100 150 200 250 300 350 400 450 500 550
T T "II T
17.60 17.80 18.00 18.20
131LB.D 5080302.M Mon Mar 18 08:30:11 2002 Page 5
NYC-WTC_000010481
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