NYC 9/11 Public Portal Document
Library Search Compound Report
pata File C:\MSDCHEM\1\DATA\030402\0131LB.D Vial: 5
Acq On 4 Mar 2002 1:32 pm Operator: McLean
Sample 1/31 Inst : Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator)
Title : Quantitation For Method 508gcscan
Library : C:\DATABASE\WILEY7N.L
Peak Number 2 Cyclohexasiloxane, dodecame... Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
15.14 0.70 ug/L 276266 Naphthalene-d8 13.05
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclohexasiloxane, dodecamethyl-... 444 C12H3606Si6 000540-97-6 91
2 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 90
3 METHYL 2,3-BIS(TRIMETHYLSILYLOXY... 341 C16H27DO4S12 000000-00-0 40
4 Cyclohexasiloxane, dodecamethyl-... 444 C12H3606Si6 000540-97-6 32
Abundance Scan 1330 (15.139 min): 0131LB.D (-) m/z 73.10 100.00%
73
5000
341
147
m/z->
Abundance
0- -+45
50 100
117
150
If Ji
200
179 207
250 300
251
350 400
r i • ■ ■ • i
429 14.80 15.00 15.20 1540
m/z 341.00 36.20%
#352523: Cyclohexasiloxane, dodecamethyl- $$ Dodecamethylc...
73
341
429
5000
14.80 15.00 15.20 15.40
m/z 147.10 15.88%
147
45 117 I 207 267 311[ 397,
0- IIm*
m/z->
Abundance
—g 100 150 200 250 300 350
#352522: Cyclohexasiloxane, dodecamethyl-
400
73
’111’1/11/8 14441144489
14.80 15.00 15.20 15.40
5000 m/z 342.00 12.34%
341
429
147
45 117 7 m, 177 297 237 271 311 367 397
; 1
0* ’.8 • ■ i 1 P -r PI 11 r"dr 1-1 f 14 "I6****
miz—> 50 100 150 200 250 300 350 400
Abundance#289709: METHYL 2,3-BIS(TRIMETHYLSILYLOXY)-5-DEUTEROPHEN Y
73 180 TI T T l ‘ ‘ ‘ I
14.80 15.00 15.20 15.40
m/z 429.10 12.29%
5000
341
45
0 1 • t 1 TT—T 1222
, 106 149 268 310, .......... ’I T T T T
miz-> 50 100 150 200 250 300 350 400 14.80 15.00 15.20 15.40
0131LB.D 5080302.M Mon Mar 18 08:30:10 2002 Page 4
NYC-WTC_000010480
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