GCMS analysis report for sample AE01511, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report : C: \MSDCHEM\1\5973N\02FEB21\01511.D • ’ Data File Vial: 2 Acq On : 21 Feb 2002 4:01 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.96 0.29 ug/L 123851 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 45 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 45 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 36 4 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 Abundance Scan 229 (5.959 min): 01511.0 (-) m/z 73.10 100.00% 73

5000 43

0- L 1''1111'0010111100m31'1 —on1—E100118UO"Z"ITUZTIIT 5.60 m/z 5.80 43.10 6.00 6.20 . 28.51% 6.40

niz-> Abundance

5000 10 20 30 40 50 60 70 80 90 1(X) 110 120 130 140 150 160 170 180 #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p...

27 55 43 73

.1 , 87 113 174 J ■ ' I ' ' • ‘ I ' ' ‘ ' I 1 1 ■ ‘ I ‘ 5.60 m/ z 5.80 45.00 6.00 6.20 12.25% 6.40

0- mmpp ‘i"'" । ““i1 1u—1—001—pP200—0mmm2T niz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-yIpropyl ester 73 5.60 5.80 6.00 6.20 6.40 5000 m/z 41.10 9.57% 43 27 87 0- mmmHm 55 i “ “ i ■" ’14 113 ’}’2’111111’111913131111776——101712""TT[’ 174 n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #4814: Silane, tetramethyl- 73 560 5.80 6.00 6.20 6.40 m/z 74.00 7.06%

5000

45 15 I 53 88 0- ' i‘ ' i'»'■ i n't. i.'.'-'i'i... .| / ' ■ i ■“11' ■ ■11 “ “ i “ “ i" ■ ‘i1" ■ i ■ ■ ■ ■ i ■ i ■ ■" i “' ■ i' ' 1 I 1 ' ' 1 I r rnfe-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20 6.40

01511.D HP022102.M Mon Feb 25 10:55:17 2002 Page 5

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