NYC-WTC_000004149
Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Document / 12 pages
GCMS calibration table with surrogate recovery data, Feb 16, 2002
Machine-extracted title · confidence 90%Calibration table page listing internal standards and response factors for GCMS analysis.
NYC-WTC_000009629–000009640Folder label: “GCMS X 1/14/02 A 3/4/02”
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NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C : \HPCHEM\ 1 \DATA\ FEB15 02\1137.D Vial: 10 Acq On : 16 Feb 2002 12:12 am Operator: 209 GALOS Sample : gc/ms scan 1/16 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L **************** * * * * ************************************************* Peak Number 6 1,3-Benzodioxole, 5-[3-acetami Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
43.03 0.34 ug/1 38569 Perylene-d12 38.09
Hit# of 5 Tentative ID MW MolForm CAS# Qual /5- [3-acetaminopro 221 C12H15NO3 1 1,3-Benzodioxole, 000000-00-0 9 2 Pentanal, (4-nitr ophenyl) hydrazone 221 C11H15N3O2 005873-64-3 9 3 Indole, 2-benzoyl 221 C15H11NO 001022-86-2 9 4 Propanedioic ac , bis(trimethylsil 248 C9H20O4Si2 018457-04-0 9
0 Abundance 7 Scan 4138 (43.028 min): 1137.D (-) 73 147 221 5000 281 355 40 42.60 42.80 43.00 43.20 43.40
m/z-> — 7 191 | | 253 | ! 1*1+44*1441114*1**1+8**24** 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 __ m/z 73.Q0 95.63% Abundance #27829: 1,3-Benzodioxole, 5-[3-acetaminopropyl]- 221
73 135 162 5000 42.60 42.80 43.00 43.20 43.40 m/z 220 65.97% 49 104119 4 1 204 mpmmmmmmpppp •41 * ‘ * 14 * ’ * I T T miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #77808, Pentaa 4-t oplenitlyorzudd 179 221 42.60 42.80 43.00 43.20 43.40 5000 131 m/z 281.00 41.60% 64 105 151 90 mfe-> 11111110un1nt5‘1— i 9 OT0u01901Eum01000I6001 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 vPWAM WWwyw Abundance #27891: Indole, 2-benzoyl- 221 42.60 42.80 43.00 43.20 43.40 144 m/z 207.00 33.19% 77 5000 vMVW MAWM 105 204 165 “ i1' “ i ■ ■ ■ ■ । ■ * ■ ■ । “1 > “ ■ ‘ । - TIPPmmmmpt 11 “ ' i “ " i “ “ i' m/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 42.60 42.80 43.00 43.20 43.40
1137.D GCMS0208.M Mon Mar 04 15:10:29 2002 Page 6
NYC-WTC_000009639
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NYC-WTC_000009639Source: NYC Law Department, mirrored locally
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