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Document / 3 pages

GCMS calibration table with surrogate recovery data, Feb 13, 2002

Machine-extracted title · confidence 90%

Calibration table page listing internal standards and response factors for GCMS analysis.

NYC-WTC_000009591–000009593

Folder label: “GCMS X 1/14/02 A 3/4/02

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Scanned page image, NYC-WTC_000009592
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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\FEB13 02\94 0.D Vial: 48 Acq On : 13 Feb 2002 2:15 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 14 9:42 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13' 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 25.82 178 459 N.D. 34) Anthracene 25.82 178 459 N.D. 35) Di-n-butylphthalate 27.72 149 10255 N.D. 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 32.25 149 193 N.D. 41) Benzo(a)anthracene 33.89 228 3621 N.D. 42) Bis(2-ethylhexyl)phthalate 34.02 149 1446 N.D. 43) Chrysene 33.89 228 3740 N.D. 45) Di-n-Octylphthalate 35.77 149 812 N.D. 4 6) Benzo(b)fluoranthene 36.90 252 2374 N.D. 47) Benzo(k)fluoranthene 36.96 252 2986 N.D. 48) Benzo(a)pyrene 37.91 252 1433 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 5 0) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 43.60 276 695 N.D.

(#) = qualifier out of range (m) = manual integration 940.D GCMS0208.M Thu Feb 14 09:43:59 2002 Page 2

NYC-WTC_000009592

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NYC-WTC_000009592Source: NYC Law Department, mirrored locally

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