GCMS sample results, AE00897, Feb 26, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\ FEB1102\897.D vial: 35 Acq On : 12 Feb 2002 9:13 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.23 0.39 ug/1 28829 1,4-Dichlorobenzene-d4 12.35

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 36 2 1,3-Dioxolane; 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 3 Silane/ tetramethyl- 88 C4H12Si 000075-76-3 9 4 N-Ethyl formamide _ _________ 73 C3H7NO _000627-45-2 5 Abundance Scan 347 (8.227 min): 897.D (-) m/z 73.00.... 100.00% 73

5000 43 i ■ ' ‘ ' i ' ■ • • i ‘ r 1 1 1 1'' 1 ■' I 1 1

m/z-> ‘ 'T • • » ' | • r • » J ■ 10 20 30 11 40 50 60 70 80 87 l-r-n-rT-rVy-rT-rT-j-TT-rTYT-rT-ryT-T 90 100 110 120 7.80 rn/z 8.00 43.05 8.20 8.40 8.60 38.96% Abundance #63572:3-Pentanol, 3-methyl- 73

5000 55 7.80 8.00 8.20 8.40 8.60 45 87 m/z 44.95 15.86% 27 ............ , ,, ... ■ i ■ 1 ‘'''i ■ I . m/z-> Abundance 10 20 30 08300 40 50 60 70 D. 908 22 bremo5 C,S4 80 ' 90 ’’100 ’110’120 73 i ■ ‘ ‘ 1 i ‘ ' 7.80 8.00 8.20 8.40 8.60 5000 m/z 41.0.5 13.86% 45 36 55 67 109115 ■ ■ i ' ■ ■ 1 i ■ ■ ■ ■ i ■ 1 ■ ■ । ■ 1 ‘ ' i ■ ■ 1 • i ■ ■ ■ ■ । ■ 1 ■ ■ i 1 1 1 1 i 1 1 1 1 i 1 1 1 1 i 1 1 1 1 i 1 1 m/z-> Abundance 10 20 30 40 50 60 70 #62932: Silane, tetramethyl- 73 80 90__ 100 .110 120 I ■ 1 ■ ■ i ■ ' 7.80 8.00 J. MJ.... 8.20 8.40 8.60 m/z 39.05 7.38% 5000

45 15 , ,1 53 59 88 • • । * i । i ■ . i । . । — ■ ■ ।' ■ ■ ■ । ■ ■ ■ ■ । ■ ■ ■' । ‘ ■11 ■ ■ 1*1+* I ’ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 7.80 8.00 8.20 8.40 8.60

897.D GCMS0208.M Wed Feb 20 09:51:30 2002 Page 1

NYC-WTC_000009484