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GCMS analysis results for sample AE03251, March 2002

Machine-extracted title · confidence 95%

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03251 conducted on March 15, 2002.

NYC-WTC_000006206–000006225

Folder label: “GCMS X 2/12/02 A 3/01/02

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Scanned page image, NYC-WTC_000006223
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document X MpulL I\CDUA

Data File : C:\MSDCHEM\1\5973N\02MAR01\03251.D Vial: 6 ' Acq On : 1 Mar 2002 8:07 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 12 1,2-Phenylene diisothiocyanate Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.13 ug/L 86828 Phenanthrene -dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Phenylene diisothiocyanate 192 C8H4N2S2 071105-17-4 53 2 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2 000000-00-0 49 3 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 45 4 1,5-Naphthalenedithiole 192 C10H8S2 000000-00-0 45 Abundance Scan 1675 (22.283 min): 03251 .D (-) m/z 192.10 100.00% 192

s.. 5000

43 70 82 96 146 160 22.00 22.20 22.40 22.60 0 TTITTTTTTTTPTHTT bp I’’ 00000000072 —0010001/0002700011 — m/z 191.00 22.13% /z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102107:1,2-Phenylene diisothiocyanate 192

5000 64 ...... II..... N, 22.00 22.20 22.40 22.60 75 90 134 m/z 146.10 14.13%

m/z—> 0 " i " " r " ' i' —’,.427. 107 ■ i1' " i1 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 160 TTIPTTTTTTTTTTTTTTTTTTTTT

Abundance #102494: N-(2-methylprop-2-enyl)-2-nitrobenzenamine 192 77 151 130 22.00 22.20 22.40 22.60 93 104 m/Z 193.00 14.09% 5000 119 a 177 0 i ‘■ i ■'"i""i "11' Tp-r III 1111 ' i" " r ' " i" ‘11" " i "11" /z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ............... . Abundance #88409: N-perdeuteriobenzylideneaniline 192 22.00 22.20 22.40 22.60 m/ z 96.00 13.68%

5000 82

54 110

m/z—> 30 0 . ................... . '' i ■" ' i'' " i 94 "I'll.,... 160 n f" " I" " I " " I' 1 11... 11.. h' 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 U 22.00 22.20 22.40 22.60

3251.D HP022102.M Mon Mar 04 12:33:49 2002 Page 14

NYC-WTC_000006223

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NYC-WTC_000006223Source: NYC Law Department, mirrored locally

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