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GCMS analysis results for sample AE02783, Mar 11, 2002

Machine-extracted title · confidence 90%

Laboratory report listing unknown compounds and surrogate recovery data for sample AE02783.

NYC-WTC_000005525–000005534

Folder label: “GCMS X 2/6/02 A 3/1/02

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Nvc or Pudic Portal Document (QT Reviewed) Quantitation Report

. \HPCHEM\1\DATA\MAR0102\2783 .D Vial: 17 Data p., 2 Mar 2002 12:06 am Operator: Acq 0, 1 gc/ms scan 2/6 Inst : GC/MS 209 Multiplr: 1.00 Samp] : Miscgration Params: GOOFY. P MS. Time: Mar 5 10:30 2002 4Quant Results File: GCMS0208.RES Q Jant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.31 152 333626 20.00 ug/1 -0.04 10) Naphthalene-d8 15.95 136 1286407 20.00 ug/1 -0.04 17) Acenaphthene-diO 21.27 164 686855 20.00 ug/1 -0.04 29) Phenanthrene-diO 25.71 188 1002899 20.00 ug/1 -0.05 38) Chrysene-dl2 33.78 240 709253 20.00 ug/1 -0.06 44) Perylene-dl2 38.05 264 490733 20.00 ug/1 -0.07

System Monitoring Compounds 37) 2,4-DDD 30.79 235 61116 5.84 ug/mL 0.29 Spiked Amount 5.000 Recovery = 116.80%

get Compounds Qvalue -2y s-ni-roso-dimethyl amine 2 bis (2-cnioroethyl) ether 0.00 74 0 N.D. 33 1 3-Dihlorobenzene 0.00 _ 93 0 N.D. 7 1 4-Dihlorobenzene 0.00 146 0 N.D. 0.00 146 0 N.D. 2 1‘2-Diclorobenzene 0.00 146 - 2, 2 ’ -O%is (1-Chloropropan 0 N.D. 0.00 45 0 N.D. gy N-Nitrodi-n-propylamine 0.00 70 0 N.D. g\ Hexachloethane 0.00 117 0 N.D. . Nitrobenne 0.00 77 t Isophoro 0.00 13) his (2-cnpethoxy) methane 0.00 82 93 0 0 N.D. N.D. 0 N.D. _ 1 2,4-Trlorobenzene 0.00 18) Naphthale g) Hexachlor adiene 16.01 0.00 180 128 225 483 0

0 N.D. N.D. N.D. - . Hexachlorlopentadiene 0.00 237 0 19) 2-chloronslalene 0.00 162 0 N.D. N.D. 4. DimethylP"ate 20) 2 6-Dinltrene 21) —' —hhylt 0.00 0.00 163 165 0 0 N.D. N.D.

233 AC“Tapnehens. 0.00 0.00 152 153 0 0 N.D. N.D. 22 , 4-chloroP 0.00 22.74 nyl ether 0.00 165 149 204 0 179 N.D. N.D. 0 N.D. 29) Fluorene , 1 ; 0.00 166 0 N.D. 28) Azobenzen _ enylhyd 0.00 77 0 N.D. ahe qualifier Ange (m) = manual integration 2783.D GCMS020 - te Mar 05 10:31:24 2002

NYC-WTC_000005527

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NYC-WTC_000005527Source: NYC Law Department, mirrored locally

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