DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB27\0201B.D Vial: 1 Acq On : 27 Feb 2002 10:33 am Operator: Sample : lab blank 2/1 Inst : Instrumen Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 7 5,6-INDOLEDIOL Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

20.00 0.06 ug/L 43494 Acenaphthene-dl0 18.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 5,6-INDOLEDIOL 149 C8H7NO2 000000-00-0 47 2 O-DIMETHYLAMINOBENZALDEHYDE $$ B... 149 C9H11NO 000579-72-6 43 3 1,2-Benzenedicarboxylic acid, mo... 222 C12H1404 000131-70-4 40 4 2-METHYL-3-INDAZOLONE-N-D1 149 C8H7DN20 054120-67-1 28 Abundance Scan 1473 (20.002 min): 0201 B.D (-) m/z 149.00 100.00% 149

5000 177 ....... ............... /........................ 51 65 76 93 105 19.60 19.80 20.00 20.20 20.40 01 ■i 1r=- s-, । J, 1111. J. । iL .. ।.,.. L, 11 — m/z 177.00 24.62% m/z-> :20 40 60 80 100 120 140 160 180 200 220 Abundances #45075:5,6-INDOLEDIOL 149

5000 103 19.60 19.80 20.00 20.20 20.40 m/ z 150.00 20.60% 50 65 76 92 120

/z-> 0- 20 27 40 L4 60 80 100 I , , . I' . 120 11*7*1 1 1 ’ 1 1 1+’I’’I 140 160 180 200 220 Abundance #45220: O-DIMETHYLAMINOBENZALDEHYDE $$ Benzaldehyde, 2-(di... 149 ..... .................

44 120 19.60 19.80 20.00 20.20 20.40 106 77 132 m/z 176.10 14.52% 5000 91

0 । > . . . ।1 1 ' । 1 ■ 1 ■ i ‘ ■ r ■ । 1 1 1 ■ i 1 1 m/z- > 20 40 60 80 100 120 140 160 180 200 220 Abundance #147069:1,2-Benzenedicarboxylic acid, monobutyl ester 149 19.60 19.80 20.00 20.20 20.40 m/z 105.00 13.37%

5000

65 167 50 | 76 93 105 122 I | 222 m/z—> 0-T 1101) 40 60 — ‘I --- L 19.60 19.80 20.00 20.20 20.40 20 80 100 120 140 160 180 200 220

3201B.D HP022102.M Thu Feb 28 08:46:40 2002 Page 9

NYC-WTC_000004957