DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004935–000005145

Folder label: “GCMS X 2/1/02 A 2/27/02”

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NYC 9/11 Public Portal Document Library searen compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB27\02454 .D Vial: 5 Acq On : 27 Feb 2002 6:38 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C : \DATABASE\WILEY7N. L

Peak Number 8 6-Methoxy-2-benzoxazolinone... Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T. 27.98 0.08 ug/L 59639 Chrysene-dl2 30.50 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 6-Methoxy-2-benzoxazolinone $$ 2... 165 C8H7NO3 000532-91-2 59 2 3-Methoxyphenyl isothiocyanate 165 C8H7NOS 003125-64-2 45 3 7-Methyl-6-oxo-l,2,3,4-tetrahydr... 165 C8H11N30 026955-14-6 45 4 l-Phenoxy-4-phenylthio-butane $$... 258 C16H180S 059950-11-7 38 Abundance Scan 2180 (27.984 min): 02454.D (-) m/z 165.10 100.00% 165

5000 , /.......... 109 308 41 55 79 95 | 27.60 27.80 28.00 28.20 28.40

m/z-> 0-। ■ i < ■ ■ । । 40 | I LL ............... ............. । 1 'Tr‘ 1 ■ 1 1 1 ■ 1 1 ■ 1 1 1 1 1 1 60 80 100 120 140 160 180 200 220 240 260 280 300 251 I +H m/z 109.10 16.45% Abundance #65759: 6-Methoxy-2-benzoxazolinone $$ 2-Benzoxazolinone, ... 165 150 / 5000 106 1 I ' 1 ' ' 1 1 ' I 1 ' ' ' I ' 1 27.60 27.80 28.00 28.20 28.40 52 80 66 122 m/z 166.10 14.52% | 136 O-TT TIT ,• I' I. 1 Illi1 ,' I, I I 1 1 ■ > II , ’■ ,' ■ ■ i ■' ■ > ।• 11 ■ ■ । । ■ j ■ ■ ■ -1 > ■ - ■ i > ■ । । ■ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #65729: 3-Methoxyphenyl isothiocyanate 1$5 ,............... 27.60 27.80 28.00 28.20 28.40 77 m. Z 55.00 11.30% 5000 63 122135 92 I 109 OTPT —PP, 11 i l । . m/z- > 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #65801: 7-Methyl-6-oxo-1,2,3,4-tetrahydro-6H-pyrimido[1 ,2-... 165 ■ i ■ ' AAM.... I " 27.60 27.80 28.00 28.20 28.40 m/ z 3 08.20 11.18%

5000 110 137 150

0— I ■ ' *1 1 m/z- > 40 60 80 100 120 140 160 180 200 220 240 260 280 300 27.60 27.80 28.00 28.20 28.40

02454.D HP022102.M Thu Feb 28 08:47:34 2002 Page 10

NYC-WTC_000005099

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NYC-WTC_000005099Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999