DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Z Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\FEB2 702\CALI 0 A.D Vial: 2 Acq On 28 Feb 2002 10:13 am Operator: Sample Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 5 12:28 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) l,4-Dichlorobenzene-d4 12.32 152 312390 20.00 ug/1 -0.04 10) Naphthalene-d8 15.96 136 1228224 20.00 ug/1 -0.04 17) Acenaphthene-diO 21.28 164 665220 20.00 ug/1 -0.04 29) Phenanthrene-diO 25.72 188 996521 20.00 ug/1 -0.05 38) Chrysene-dl2 33.79 240 705075 20.00 ug/1 -0.06 44) Perylene-dl2 38.07 264 496765 20.00 ug/1 -0.06 System Monitoring Compounds 37) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.94 74 155449 12.44 ug/1 # 72 3) bis(2-Chloroethyl)ether 11.72 93 243225 11.85 ug/1 94 4) 1,3-Dichlorobenzene 12.22 146 251571 10.29 ug/1 99 5) 1,4-Dichlorobenzene 12.36 146 253671 10.18 ug/1 99 6) 1,2-Dichlorobenzene 12.89 146 236691 10.00 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 13.20 45 351574 11.31 ug/1 99 8) N-Nitroso-di-n-propylamine 13.59 70 163839 11.15 ug/1 # 87 9) Hexachloroethane 13.73 117 93327 9.36 ug/1 98 11) Nitrobenzene 14.01 77 244046 9.66 ug/1 95 12) 1sophorone 14.65 82 455763 10.68 ug/1 98 13) bis(2-Chloroethoxy)methane 15.33 93 290980 10.95 ug/1 98 14) 1,2,4-Trichlorobenzene 15.84 180 204830 9.74 ug/1 97 15) Naphthalene 16.02 128 660724 10.10 ug/1 99 16) Hexachlorobutadiene 16.56 225 107322 8.53 ug/1 99 18) Hexachlorocyclopentadiene 18.76 237 75736 77. 95) ug/1 98 19) 2-Chloronaphthalene 19.53 162 398647 10.05 ug/1 97 20) Dimethylphthalate 20.62 163 462494 10.01 ug/1 100 21) 2,6-Dinitrotoluene 20.83 165 106678 10.19 ug/1 90 22) Acenaphthylene 20.80 152 589234 10.28 ug/1 100 2 3) Acenaphthene 21.37 153 409660 10.23 ug/1 98 24) 2,4-Dinitrotoluene 22.00 165 139158 10.49 ug/1 # 81 25) Diethylphthalate 22.75 149 456626 9.51 ug/1 97 26) 4-Chlorophenyl-phenylether 22.90 204 204077 9.88 ug/1 99 27) Fluorene 22.88 166 439795 10.06 ug/1 100 28) Azobenzen/ 1,2-Diphenylhyd 23.38 77 477956 9.47 ug/L # 87

(#) = qualifier out of range (m) = manual integration CAL10A.D GCMS0208.M Thu Mar 07 10:52:54 2002 Page 1

NYC-WTC_000004708