Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
NYC-WTC_000004149–000004492Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\LBD.D Vial: 38 Acq On : 29 Dec 2001 7:39 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 6 Benzeneethanamine, N-[(pentafl Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
22.79 1.09 ug/1 548427 Phenanthrene-dl0 24.98
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Benzeneethanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 46 2 N- (Trifluoracetyl) -0,0',0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 43 3 N-(Trifluoroe cetyl)-0,0',0''-tris(t 481 C19H34F3NO4Si3 000000-00-0 43 4 Benzoic acid, 2,6-bis[(trimethylsil 370 C16H30O4Si3 __ 003782-85-2 25 Abundance Scan 1933 (22.788 min): LBD.D (-) m/ z 73.00 100.00% 73
5000 147 ............. ...... 94 355 221 281 | 22.40 22.60 22.80 23.00 23.20 ; 45 0- T—' I |^ 18t | ‘ 117 191, [ 249, J' । 32/ 4 . 401 m/z 147.00 26.18% m/z-> 50 100 150 200 250, 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 355
, । . , , -Q , . , < । \ , । I i i i । i i 5000 22.40 22.60 22.80 23.00 23.20 45 i m/z 355.0 23.20% 208 251 281 386 458 548 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58807: N-{Tnfluoracetyh)-0.0,0"tris(triethvisilylepin 73 355 22.40 22.60 22.80 23.00 23.20 5000 m/z 221.05 16.78%
45 140 184 281 480 ! 1 1 I 1 1 ' 1 I 1 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58326: N-(Trifluoroacetyl)-O,O',O’'-tr1s(trimethylsilyl)no 73 22.40 22.60 22.80 23.00 23.20 355 m/z 281.00 13.44% 5000
45 | li 120147 193 265 481 ■ 1 i • ’ 1 r 1 | i ■ ■ ■ I ■ < m/z-> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00 23.20
LBD.D GCMS1126.M Mon Jan 28 11:39:23 2002 Page 6
NYC-WTC_000004202
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
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NYC-WTC_000004148
Fragmented OCR text showing dates and identifiers for a DEP GCMS record dated February 2002.
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GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
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