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DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004259
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\JAN2 502\30649.D Vial: 34 Acq On : 25 Jan 2002 9 :55 pm Operator: 209 GALOS Sample : REINJECT Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 6 3-Isopropoxy-l,1,1,7,7,7-hexam Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

20.08 5.24 ug/1 4744770 Acenaphthene-dl0 20.35

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Isopropoxy-L,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 45 2 Trisiloxane,/, 1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 38 3 4-Amino-5-imidazole carboxamide, tr 342 C13H30N4OSi3 000000-00-0 22 4 Phosphoric acid, 3-(ethoxyimino)-2- 429 C14H36NO 6 PS13 __ 055334-96-8 10 [Abundance Scan 1638 (20.085 min): 30649.D (-) m/ z 73.00 100.00% 73

5000 147 281 327 45 19.80 20.00 20.20 20,40 —1001Z— . , -I—rtii A.-| r , 1 355,383 415.. 191 221 251 0- r m/ z 147.00 37.45% miz-> 50 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 147 19.80 20.00 20.20 20.40 m/z 281.00 34.83%

m/z-> .... 50 100 .. 21..21, 327 .. 4^5, .51956* 150 200 250 300 350 400 450 500 550 Abundance #52459; Trisilxanc, 1,1.1 5,5,-besanicth-3.3-bisi(trimet 73 147 281 19.80 20.00 20.20 20.40 5000- m/z 326.90 13.92% 369 207 249 | 338 1 m/z--> 50 100 150 200 250 300 350 400 450 500 550 Abundance #48317:4-Amino-5-imidazole carboxamide, tris(trimethylsily 73 19.80 20.00 20.20 20.40 m/z 282.00 9.74% 327 5000 237 45 । I ... ..... 147 I 172 . 212 it 1.... ,,,,,,,,,,,,.... ' 1 I ' 1 miz-> 50 100 150 200 250 300 350 400 450 500 550 19.80 20.00 20.20 20.40

30649.D GCMS1126.M Mon Jan 28 12:18:18 2002 Page 6

NYC-WTC_000004259

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NYC-WTC_000004259Source: NYC Law Department, mirrored locally

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