DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB01\30642.D Vial: 5 Acq On : 1 Feb 2002 1:54 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

5.92 0.42 ug/L 180022 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 36 2 1,3-Dioxolane, 2 -(3-bromo-5,5,5-... 352 C10H16BrC13O2 000000-00-0 25 3 3-Pentanol, 3-methyl- (CAS) $$ 3... 102 C6H140 000077-74-7 25 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 223 (5.920 min): 30642.D (-) m/ z 73.10 100.00% 73

5000 43 1 ' i ' ■ ' ' i ■ ' 1 ‘ i ' 1 ' ' i 5.60 6.00 6.20 5.80

m/z—> O'. I . ■ ■ > I ' . 20 30 —lll 40 51 57 50 60 •i ‘ i‘ ' 1 । , । ] ' 1 l ' ' ‘ ' 1 70 80 ' i 90 87 100 103 110 120 m/ z 43.10 28.46% Abundance #9663:3-Pentanol, 3-methyl- 73

5000 A... M 4 5.60 5.80 6.00 6.20 55 m/z 41.10 11.07% 45 87 27 O—T J, ! 39,1 1 1 1 ■ ■ ' ' I ' 1 1,1 i ' 1 1 ■' i ' i ■ ■ | . p—r I I | 1 1 .! | I I I I | I

m/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #299410: 1,3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dim... 73 .... JX 1..... ' 5.60 5.80 6.00 6.20 ''' 5000 m/z 45.10 10.97% 45 36 i I 55 67. 109114 0-m----- l ' i j .-i1!LL 1 1 *■' ’ ■ I 1 ' I ' K ' I ' ' 1 ' 1 1 1 1 ‘ I rR—mi"l ri i । i i m/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #9667:3-Pentanol, 3-methyl- (CAS) $$ 3-Methyl-3-pentanol... 73 5.60 5.80 6.00 6.20 '' ' m/z 71.10 7.65% 55 5000 43

87 0—PPPPo T+ trormtr ^-T' ' ' 11 ■ -------------- 1 ■ i ■ 1 ■ ■ i ■ ' ■ ■ i ■ ' ' ■ i ■ ' ' ■ । m/z— > 20 30 40 50 60 70 80 90 100 110 120 5.60 5.80 6.00 6.20

30642.D SCAN508.M Mon Feb 04 08:41:18 2002 Page 3

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