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GCMS analysis results for sample AE01942 with surrogate data, Feb

Machine-extracted title · confidence 50%

Laboratory report for sample AE01942 showing GCMS analysis of unknown compounds and surrogate recovery on February 15, 2002.

NYC-WTC_000003864–000003871

Folder label: “GCMS X 1/28/02 A 2/8/02”

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\FEB0802\1942.D Vial: 22 Acq On 9 Feb 2002 5:44 am Operator: 209 GALOS Sample GC/MS SCAN 1/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.343 790 795 808 rVB 866457 2067395 73.62% 15.084% 2 15.988 1186 1192 1207 rBV 1300816 2558778 91.12% 18.669% 3 21.303 1765 1771 1788 rBV 1373688 2808281 100.00% 20.489% 4 25.755 2249 2256 2267 rBV2 1287607 2685783 95.64% 19.595% 5 30.832 2804 2809 2815 rBV 138592 261137 9.30% 1.905%

6 33.825 3128 3135 3152 rBV 898687 1954059 69.58% 14.257% 7 38.112 3593 3602 3619 rBV2 463031 1370707 48.81% 10.001%

Sum of corrected areas: 13706140

1942.D GCMS0208.M Thu Feb 14 15:01:46 2002

NYC-WTC_000003869

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NYC-WTC_000003869Source: NYC Law Department, mirrored locally

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