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GCMS analysis results for sample AE01937 with surrogate data, Feb

Machine-extracted title · confidence 50%

Laboratory report for sample AE01937 showing GCMS analysis of unknown compounds and surrogate recovery on February 15, 2002.

NYC-WTC_000003839–000003847

Folder label: “GCMS X 1/28/02 A 2/8/02

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Scanned page image, NYC-WTC_000003844
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\FEB0802\1937.D Vial: 17 Acq On 9 Feb 2002 12:53 am Operator: 209 GALOS Sample GC/MS SCAN 1/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.345 790 795 806 rBV 619892 1565938 76.13% 15.558% 2 15.990 1186 1192 1210 rBV 991330 1939157 94.28% 19.266% 3 21.305 1765 1771 1780 rBV 1033890 2056869 100.00% 20.435% 4 25.758 2249 2256 2267 rBV 929508 1971537 95.85% 19.588% 5 27.713 2464 2469 2475 rVB 12653 23746 1.15% 0.236%

6 30.835 2804 2809 2814 rBV 103819 191986 9.33% 1.907% 7 33.818 3128 3134 3152 rBV2 602234 1363029 66.27% 13.542% 8 38.105 3593 3601 3616 rBV2 322460 952968 46.33% 9.468%

Sum of corrected areas: 10065230

1937.D GCMS0208.M Thu Feb 14 15:00:24 2002

NYC-WTC_000003844

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NYC-WTC_000003844Source: NYC Law Department, mirrored locally

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