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GCMS analysis results for sample AE01939 with surrogate data, Feb

Machine-extracted title · confidence 50%

Laboratory report for sample AE01939 showing GCMS analysis of unknown compounds and surrogate recovery on February 15, 2002.

NYC-WTC_000003856–000003863

Folder label: “GCMS X 1/28/02 A 2/8/02”

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\FEB0802\1939.D Vial: 19 Acq On 9 Feb 2002 2:50 am Operator: 209 GALOS Sample GC/MS SCAN 1/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.348 790 796 811 rVB 705674 1746296 74.08% 15.483% 2 15.993 1187 1193 1206 rBV 1045649 2156919 91.49% 19.124% 3 21.308 1765 1772 1784 rBV 1146247 2357470 100.00% 20.902% 4 25.751 2250 2256 2268 rBV 1057369 2217398 94.06% 19.660% 5 30.828 2805 2809 2815 rVB 112829 213035 9.04% 1.889%

6 33.821 3129 3135 3154 rBV 722626 1543920 65.49% 13.689% 7 38.108 3594 3602 3616 rBV2 364303 1043631 44.27% 9.253%

Sum of corrected areas: 11278669

1939.D GCMS0208.M Thu Feb 14 15:01:21 2002

NYC-WTC_000003861

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NYC-WTC_000003861Source: NYC Law Department, mirrored locally

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