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VOCs GC/MS lab blank results, Jan 16 2002

Machine-extracted title · confidence 95%

Gas chromatography mass spectrometry analysis report for a laboratory blank testing volatile organic compounds on January 16, 2002.

NYC-WTC_000003343–000003381

Folder label: “524 1/22/02”

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NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed) .~

Data File : C:\HPCHEM\1\DATA\02JAN16\0116R40.D Vial: 3 - Acq On : 16 Jan 2002 11:03 am Operator: 201-wb Sample : ref 40 Inst : GC/MS Ins Misc Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Feb 5 12:56 2002 Quant Results File: HP010702.RES"

Quant Method : C:\HPCHEM\1\METHODS\HP010702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Fri Jan 25 14:13:49 2002 Response via : Initial Calibration DataAcq Meth : HP010702

Compound R.T. Qlon Response Conc Unit Qvalue ------------------------------------------------------------------------- 34) 2-CHLOROETHYL VINYL ETHER 17.25 63 533672 44.38 ug/L 96 35) METHYL ISO-BUTYL KETONE 17.33 58 270005 36.74 ug/L 90 36) CIS-1,3-DICHLOROPROPENE 17.86 75 2038384 46.72 ug/L 99 - 37) TOLUENE 18.62 91 5208489 40.68 ug/L 100 „ 38) TRANS-1,3-DICHLOROPROPENE 18.90 75 1693080 50.89 ug/L 98 -- 39) 1,1,2-TRICHLOROETHANE 19.28 97 884977 39.80 ug/L 96 40) TETRACHLOROETHENE 20.07 166 1409172 40.87 ug/L 99 41) 1,3-DICHLOROPROPANE 19.81 76 1751488 40.69 ug/L 97 42) DIBROMOCHLOROMETHANE 20.50 129 1340794 44.21 ug/L 97 43) 1,2-DIBROMOETHANE 20.96 107 946493 42.48 ug/L 100 44) CHLOROBENZENE 21.83 112 3331632 38.68 ug/L 99 45) 1,1,1,2-TETRACHLOROETHANE 21.88 131 1333543 41.14 ug/L 98 46) 2-HEXANONE 19.18 43 598592 36.68 ug/L 99 47) ETHYLBENZENE 21.88 91 6556673 40.94 ug/L 100 48) P & M-XYLENE 22.04 106 4411917 82.96 ug/L 100 49) O-XYLENE 23.01 91 5375637 44.13 ug/L 98 50) STYRENE 23.07 104 3453791 44.50 ug/L 98 51) 1,1,2,2-TETRACHLOROETHANE 24.09 83 983149 40.47 ug/L 98 53) BROMOFORM 23.92 173 635541 44.18 ug/L 95 54) ISOPROPYLBENZENE 23.73 105 5577567 43.74 ug/L 98 55) 1,2,3-TRICHLOROPROPANE 24.42 110 301732 37.66 ug/L 92 56) N-PROPYLBENZENE 24.60 91 7390406 41.51 ug/L 99 57) BROMOBENZENE 24.84 156 1357649 40.16 ug/L 99 58) 1,3,5-TRIMETHYLBENZENE 24.91 105 5211932 43.33 ug/L 100 59) 2-CHLOROTOLUENE 25.09 91 5276178 42.35 ug/L 98 60) 4-CHLOROTOLUENE 25.16 91 4447531 38.85 ug/L 97 _,.~. 61) TERT-BUTYLBENZENE 25.71 119 4450690 43.22 ug/L 98 62) 1,2,4-TRIMETHYLBENZENE 25.80 105 5269099 42.53 ug/L 99 - 63) SEC-BUTYLBENZENE 26.17 105 6013064 43.76 ug/L 98 64) P-ISOPROPYLTOLUENE 26.43 119 4730248 45.55 ug/L 97 -- 65) 1,3-DICHLOROBENZENE 26.78 146 2446278 40.96 ug/L 98 66) 1,4-DICHLOROBENZENE 27.00 146 2465617 40.21 ug/L 97 67) N-BUTYLBENZENE 27.32 91 5329319 44.81 ug/L 99 68) 1,2-DICHLOROBENZENE 27.86 146 2132871 40.54 ug/L 100 69) 1,2-DIBROMO-3-CHLOROPROPAN 29.63 157 114019 43.99 ug/L 100 70) 1,2,4-TRICHLOROBENZENE 31.93 180 1470342 46.10 ug/L 96 71) HEXACHLOROBUTADIENE 32.25 225 971559 43.08 ug/L 98 72) NAPHTHALENE 32.77 128 1969645 25.63 ug/L 100 73) 1,2,3-TRICHLOROBENZENE 33.49 180 1203572 43.88 ug/L 96 74) NITROBENZENE 29.86 77 868389 970.72 ug/L 96

(#) = qualifier out of range (m) = manual integration 0116R40.D HP010702.M Tue Feb 05 12:57:07 2002 Page 2

NYC-WTC 000003355

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NYC-WTC_000003355Source: NYC Law Department, mirrored locally

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Gas chromatography mass spectrometry analysis report for a laboratory blank testing volatile organic compounds on January 11, 2002.

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