VOCs GC/MS analysis results, Jan 14 2002

NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed)

Data File : C:\HPCHEM\1\DATA\02jan14\0114C10A.D Vial: 2 Acq On 14 Jan 2002 4:58 pm Operator: 201-wb Sample : cal 10 Inst : GC/MS Ins Misc : January 14, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Jan 14 17:36 2002 Quant Results File: HP010702.RES

Quant Method : C:\HPCHEM\1\METHODS\HP010702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Thu Jan 10 08:57:29 2002 Response via : Initial Calibration DataAcq Meth : HP010702

Compound R.T. Qlon Response Conc Unit Qvalue ------------------------------------------------------------------------- 34) 2-CHLOROETHYL VINYL ETHER 17.28 63 85456 8.96 ug/L 94. 35) METHYL ISO-BUTYL KETONE 17.37 58 51093 8.76 ug/L 87 36) CIS-1,3-DICHLOROPROPENE 17.89 75 339534 9.81 ug/L 98 37) TOLUENE 18.64 91 1027433 10.12 ug/L 100 38) TRANS-1,3-DICHLOROPROPENE 18.92 75 251422 9.53 ug/L 99 39) 1,1,2-TRICHLOROETHANE 19.30 97 173261 9.82 ug/L 96 40) TETRACHLOROETHENE 20.09 166 267873 9.79 ug/L 97 41) 1,3-DICHLOROPROPANE 19.84 76 328592 9.62 ug/L 97 42) DIBROMOCHLOROMETHANE 20.52 129 230868 9.60 ug/L 98 43) 1,2-DIBROMOETHANE 20.97 107 163926 9.28 ug/L 98 44) CHLOROBENZENE 21.86 112 676139 9.90 ug/L 96 45) 1,1,1,2-TETRACHLOROETHANE 21.90 131 252771 9.83 ug/L 94 46) 2-HEXANONE 19.20 43 115572 8.93 ug/L 93 47) ETHYLBENZENE 21.90 91 1284694 10.11 ug/L 100 48) P & M-XYLENE 22.05 106 893374 21.18 ug/L 99 49) O-XYLENE 23.03 91 1025163 10.61 ug/L 100 50) STYRENE 23.08 104 659061 10.70 ug/L 97 51) 1,1,2,2-TETRACHLOROETHANE 24.11 83 188728 9.79 ug/L 100 53) BROMOFORM 23.95 173 105789 9.17 ug/L 95 54) ISOPROPYLBENZENE 23.74 105 1051849 10.28 ug/L 100 55) 1,2,3-TRICHLOROPROPANE 24.44 110 59699 9.29 ug/L 99 56) N-PROPYLBENZENE 24.62 91 1459786 10.22 ug/L 100 57) BROMOBENZENE 24.86 156 261693 9.65 ug/L 96 58) 1,3,5-TRIMETHYLBENZENE 24.93 105 1007306 10.44 ug/L 100 59) 2-CHLOROTOLUENE 25.10 91 1054320 10.55 ug/L 98 60) 4-CHLOROTOLUENE 25.17 91 924539 10.07 ug/L 100 61) TERT-BUTYLBENZENE 25.73 119 856731 10.37 ug/L 97 62) 1,2,4-TRIMETHYLBENZENE 25.82 105 1043151 10.49 ug/L 99 63) SEC-BUTYLBENZENE 26.18 105 1127771 10.23 ug/L 100 64) P-ISOPROPYLTOLUENE 26.45 119 855281 10.27 ug/L 97 65) 1,3-DICHLOROBENZENE 26.81 146 470213 9.81 ug/L 99 66) 1,4-DICHLOROBENZENE 27.02 146 497223 10.11 ug/L 98 67) N-BUTYLBENZENE 27.33 91 968560 10.15 ug/L 99 68) 1,2-DICHLOROBENZENE 27.87 146 408062 9.67 ug/L 97 69) 1,2-DIBROMO-3-CHLOROPROPAN 29.65 157 17330 8.33 ug/L 91 70) 1,2,4-TRICHLOROBENZENE 31.95 180 234272 9.16 ug/L 95 71) HEXACHLOROBUTADIENE 32.27 225 168479 9.31 ug/L 98 72) NAPHTHALENE 32.81 128 280293 8.31 ug/L 99 73) 1,2,3-TRICHLOROBENZENE 33.52 180 199011 9.04 ug/L 95 74) NITROBENZENE 29.88 77 107928 150.39 ug/L 92

------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration 0114C10A.D HP010702.M Mon Jan 14 17:36:46 2002 Page 2

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