VOCs GC/MS analysis results, Jan 16-18 2002

NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed)

Data File : C:\HPCHEM\1\DATA\02jan16\0116C10.D Vial: 2 Acq On : 16 Jan 2002 10:18 am Operator: 201-wb Sample : cal 10 Inst : GC/MS Ins Misc Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Jan 16 10:57 2002 Quant Results File: HP010702.RES

Quant Method : C:\HPCHEM\1\METHODS\HP010702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Thu Jan 10 08:57:29 2002 Response via : Initial Calibration DataAcq Meth : HP010702

Compound R.T. Qlon Response Conc Unit Qvalue ------------------------------------------------------------------------- 34) 2-CHLOROETHYL VINYL ETHER 17.25 63 115569 10.31 ug/L 94 35) METHYL ISO-BUTYL KETONE 17.33 58 72222 10.54 ug/L 97 36) CIS-1,3-DICHLOROPROPENE 17.86 75 437692 10.76 ug/L 99 37) TOLUENE 18.62 91 1303709 10.92 ug/L 99 38) TRANS-1,3-DICHLOROPROPENE 18.90 75 331572 10.69 ug/L 99 39) 1,1,2-TRICHLOROETHANE 19.28 97 220602 10.64 ug/L 97 40) TETRACHLOROETHENE 20.07 166 355606 11.07 ug/L 97 41) 1,3-DICHLOROPROPANE 19.81 76 415090 10.35 ug/L 96 42) DIBROMOCHLOROMETHANE 20.50 129 306329 10.84 ug/L 98 43) 1,2-DIBROMOETHANE 20.96 107 215150 10.36 ug/L 99 44) CHLOROBENZENE 21.83 112 867281 10.80 ug/L 99 45) 1,1,1,2-TETRACHLOROETHANE 21.88 131 319005 10.56 ug/L 98 46) 2-HEXANONE 19.18 43 141316 9.29 ug/L 100 47) ETHYLBENZENE 21.86 91 1652702 11.07 ug/L 98 48) P & M-XYLENE 22.04 106 1130554 22.81 ug/L 98 49) O-XYLENE 23.00 91 1303908 11.49 ug/L 99 50) STYRENE 23.07 104 816794 11.29 ug/L 99 51) 1,1,2,2-TETRACHLOROETHANE 24.08 83 242000 10.69 ug/L 91 53) BROMOFORM 23.92 173 141430 10.72 ug/L 97 54) ISOPROPYLBENZENE 23.73 105 1357464 11.61 ug/L 95 55) 1,2,3-TRICHLOROPROPANE 24.41 110 74467 10.13 ug/L 98 56) N-PROPYLBENZENE 24.60 91 1897479 11.62 ug/L 100 57) BROMOBENZENE 24.84 156 336409 10.85 ug/L 96 58) 1,3,5-TRIMETHYLBENZENE 24.91 105 1284332 11.64 ug/L 98 59) 2-CHLOROTOLUENE 25.07 91 1196380 10.47 ug/L 97 60) 4-CHLOROTOLUENE 25.16 91 1284941 12.24 ug/L 98 61) TERT-BUTYLBENZENE 25.70 119 1099677 11.64 ug/L 99 62) 1,2,4-TRIMETHYLBENZENE 25.80 105 1319363 11.61 ug/L 100 63) SEC-BUTYLBENZENE 26.17 105 1486956 11.80 ug/L 99 64) P-ISOPROPYLTOLUENE 26.41 119 1119651 11.75 ug/L 97 65) 1,3-DICHLOROBENZENE 26.78 146 600087 10.95 ug/L 98 66) 1,4-DICHLOROBENZENE 26.99 146 626098 11.13 ug/L 97 67) N-BUTYLBENZENE 27.30 91 1271266 11.65 ug/L 98 68) 1,2-DICHLOROBENZENE 27.84 146 513977 10.65 ug/L 98 69) 1,2-DIBROMO-3-CHLOROPROPAN 29.62 157 24348 10.24 ug/L 83 70) 1,2,4-TRICHLOROBENZENE 31.92 180 320376 10.95 ug/L 96 71) HEXACHLOROBUTADIENE 32.23 225 228246 11.03 ug/L 99 72) NAPHTHALENE 32.77 128 398850 10.35 ug/L 100 73) 1,2,3-TRICHLOROBENZENE 33.49 180 266716 10.60 ug/L 96 74) NITROBENZENE 29.84 77 151510 184.66 ug/L 95

------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration 0116C10.D HP010702.M Wed Jan 16 10:57:28 2002 Page 2

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