VOCs GC/MS analysis results, Jan 14 2002

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Data File : C:\HPCHEM\1\DATA\02jan14\0114C10.D Vial: 2 Acq On : 14 Jan 2002 9:14 am Operator: 201-wb Sample : cal 10 Inst : GC/MS Ins Misc : January 14, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Jan 14 9:52 2002 Quant Results File: HP010702.RES

Quant Method : C:\HPCHEM\1\METHODS\HP010702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Thu Jan 10 08:57:29 2002 Response via : Initial Calibration DataAcq Meth : HP010702

Compound R.T. Qlon Response Conc Unit Qvalue ------------------------------------------------------------------------- 34) 2-CHLOROETHYL VINYL ETHER 17.26 63 125888 11.36 ug/L 93 35) METHYL ISO-BUTYL KETONE 17.33 58 71393 10.54 ug/L 91 36) CIS-1,3-DICHLOROPROPENE 17.86 75 468061 11.64 ug/L 99 37) TOLUENE 18.62 91 1316945 11.16 ug/L 100 38) TRANS-1,3-DICHLOROPROPENE 18.90 75 351954 11.47 ug/L 98 39) 1,1,2-TRICHLOROETHANE 19.29 97 229947 11.22 ug/L 97 40) TETRACHLOROETHENE 20.07 166 366087 11.51 ug/L 98 41) 1,3-DICHLOROPROPANE 19.81 76 438546 11.05 ug/L 94 42) DIBROMOCHLOROMETHANE 20.50 129 320140 11.45 ug/L 100 43) 1,2-DIBROMOETHANE 20.96 107 229000 11.15 ug/L 92 44) CHLOROBENZENE 21.83 112 870612 10.96 ug/L 98 45) 1,1,1,2-TETRACHLOROETHANE 21.88 131 329986 11.04 ug/L 96 46) 2-HEXANONE 19.18 43 157250 10.45 ug/L 99 47) ETHYLBENZENE 21.88 91 1647969 11.16 ug/L 99 48) P & M-XYLENE 22.04 106 1119038 22.82 ug/L 99 49) O-XYLENE 23.00 91 1330031 11.84 ug/L 99 50) STYRENE 23.07 104 829913 11.60 ug/L 97 51) 1,1,2,2-TETRACHLOROETHANE 24.08 83 254195 11.35 ug/L 95 53) BROMOFORM 23.92 173 148982 11.12 ug/L 96 54) ISOPROPYLBENZENE 23.73 105 1377189 11.60 ug/L 99 55) 1,2,3-TRICHLOROPROPANE 24.41 110 82312 11.03 ug/L 95 56) N-PROPYLBENZENE 24.60 91 1885824 11.37 ug/L 100 57) BROMOBENZENE 24.84 156 342846 10.89 ug/L 97 58) 1,3,5-TRIMETHYLBENZENE 24.91 105 1267014 11.31 ug/L 98 59) 2-CHLOROTOLUENE 25.07 91 1404275 12.10 ug/L 96 60) 4-CHLOROTOLUENE 25.16 91 1078399 10.12 ug/L 100 61) TERT-BUTYLBENZENE 25.70 119 1089823 11.36 ug/L 98 62) 1,2,4-TRIMETHYLBENZENE 25.80 105 1307512 11.33 ug/L 98 63) SEC-BUTYLBENZENE 26.17 105 1482225 11.58 ug/L 98 64) P-ISOPROPYLTOLUENE 26.43 119 1097149 11.34 ug/L 97 65) 1,3-DICHLOROBENZENE 26.78 146 615215 11.06 ug/L 98 66) 1,4-DICHLOROBENZENE 27.00 146 643118 11.26 ug/L 98 67) N-BUTYLBENZENE 27.30 91 1241519 11.21 ug/L 98 68) 1,2-DICHLOROBENZENE 27.86 146 532057 10.86 ug/L 99 69) 1,2-DIBROMO-3-CHLOROPROPAN 29.64 157 25271 10.47 ug/L 94 70) 1,2,4-TRICHLOROBENZENE 31.94 180 328850 11.07 ug/L 98 71) HEXACHLOROBUTADIENE 32.23 225 228835 10.90 ug/L 97 72) NAPHTHALENE 32.77 128 403525 10.31 ug/L 98 73) 1,2,3-TRICHLOROBENZENE 33.49 180 279760 10.95 ug/L 95 74) NITROBENZENE 29.84 77 165732 198.94 ug/L 95

------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration 0114C10.D HP010702.M Mon Jan 14 09:52:46 2002 Page 2

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