VOC analysis results sample AD24483, Site 524, Oct 2001

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Data File : C:\HPCHEM\1\DATA\02FEB01\0201C10A.D Vial: 15 Acq On 1 Feb 2002 8:37 pm Operator: 201-wb Sample : cal 10 Inst : GC/MS Ins Misc : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Feb 4 10:24 2002 Quant Results File: HP013102.RES

Quant Method : C:\HPCHEM\1\METHODS\HP013102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Fri Feb 01 13:18:32 2002 Response via : Initial Calibration DataAcq Meth : HP013102

Compound R.T. Qlon Response Conc Unit Qvalue ------------------------------------------------------------------------- 35) METHYL ISO-BUTYL KETONE 17.39 58 143163 8.75 ug/L 98 36) CIS-1,3-DICHLOROPROPENE 17.93 75 1034471 9.14 ug/L 98 37) TOLUENE 18.70 91 2554740 9.15 ug/L 100 38) TRANS-1,3-DICHLOROPROPENE 18.96 75 774664 8.80 ug/L 97 39) 1,1,2-TRICHLOROETHANE 19.36 97 427973 8.85 ug/L 99 40) TETRACHLOROETHENE 20.14 166 688692 8.74 ug/L 98 41) 1,3-DICHLOROPROPANE 19.88 76 835914 9.22 ug/L 98 42) DIBROMOCHLOROMETHANE 20.58 129 563719 8.48 ug/L 99 43) 1,2-DIBROMOETHANE 21.03 107 485935 8.98 ug/L 96 44) CHLOROBENZENE 21.90 112 1667842 9.16 ug/L 99 45) 1,1,1,2-TETRACHLOROETHANE 21.95 131 601782 8.89 ug/L 99 46) 2-HEXANONE 19.24 43 259837 8.43 ug/L 98 47) ETHYLBENZENE 21.94 91 3041312 9.29 ug/L 99 48) P & M-XYLENE 22.09 106 2044862 18.63 ug/L 99 49) O-XYLENE 23.07 91 2454615 9.12 ug/L 98 50) STYRENE 23.14 104 1767332 9.42 ug/L 98 51) 1,1,2,2-TETRACHLOROETHANE 24.15 83 467094 9.74 ug/L 98 53) BROMOFORM 23.99 173 287234 8.10 ug/L 99 54) ISOPROPYLBENZENE 23.80 105 2705763 9.31 ug/L 99 55) 1,2,3-TRICHLOROPROPANE 24.48 110 140075 8.99 ug/L 97 56) N-PROPYLBENZENE 24.67 91 3456128 9.43 ug/L 99 57) BROMOBENZENE 24.91 156 685917 9.16 ug/L 99 58) 1,3,5-TRIMETHYLBENZENE 24.98 105 2318361 9.32 ug/L 98 59) 2-CHLOROTOLUENE 25.16 91 2422376 10.02 ug/L 99 60) 4-CHLOROTOLUENE 25.22 91 1932609 8.74 ug/L 99 61) TERT-BUTYLBENZENE 25.78 119 2070766 9.31 ug/L 99 62) 1,2,4-TRIMETHYLBENZENE 25.87 105 2421894 9.35 ug/L 99 63) SEC-BUTYLBENZENE 26.23 105 2876228 9.52 ug/L 100 64) P-ISOPROPYLTOLUENE 26.50 119 2186042 9.35 ug/L 99 65) 1,3-DICHLOROBENZENE 26.86 146 1251671 9.28 ug/L 96 66) 1,4-DICHLOROBENZENE 27.07 146 1278205 9.43 ug/L 99 67) N-BUTYLBENZENE 27.38 91 2271800 9.43 ug/L 100 68) 1,2-DICHLOROBENZENE 27.92 146 1086158 9.21 ug/L 99 69) 1,2-DIBROMO-3-CHLOROPROPAN 29.72 157 67825 7.98 ug/L 99 70) 1,2,4-TRICHLOROBENZENE 32.01 180 693826 9.02 ug/L 99 71) HEXACHLOROBUTADIENE 32.33 225 329334 9.00 ug/L 99 72) NAPHTHALENE 32.87 128 954084 9.03 ug/L 100 73) 1,2,3-TRICHLOROBENZENE 33.58 180 541237 8.76 ug/L 96 74) NITROBENZENE 29.92 77 458924 138.28 ug/L 97

------------------------------------------------------------------------- (##) = qualifier out of range (m) = manual integration 0201C10A.D HP013102.M Mon Feb 04 10:24:50 2002 Page 2

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