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← Document results/DEP Box 04/524 11/9/01
Document / 80 pages

VOC analysis results, sample AD26987, Nov 2001

Machine-extracted title · confidence 100%

Lab report for sample AD26987 showing VOC results with manual entry started November 9, 2001.

NYC-WTC_000000920–000000999

Folder label: “524 11/9/01

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Scanned page image, NYC-WTC_000000926
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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\O1NOV9\1109C10.D Vial: 6 Acq On 9 Nov 2001 10:42 am Operator: Sample : cal 10 Inst : GC/MS Ins Misc Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Nov 9 11:27 2001 Quant Results File: HP110101.RES

Quant Method : C:\HPCHEM\1\METHODS\HP110101.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Fri Nov 02 15:17:46 2001 Response via : Initial Calibration DataAcq Meth : HP110101

Internal Standards R.T. Qlon Response Conc Units Dev(Min) ------------------------------------------------------------------------- 1) 1,4-DIFLUOROBENZENE 14.39 114 642409 5.00 ug/L -0.05 22) CHLOROBENZENE-D5 20.98 117 574809 5.00 ug/L -0.05 50) 1,4-DICHLOROBENZENE-D4 26.14 152 265625 5.00 ug/L -0.05 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 13.60 65 199520 5.26 ug/L -005 Spiked Amount 5.000 Recovery = 105.20% 3) 4-BROMOFLUOROBENZENE 23.55 174 192071 5.75 ug/L -0®.05 Spiked Amount 5.000 Recovery = 115.00% `i 23) TOLUENE-D8 17.71 98 870878 5.02 ug/L -0.03 Spiked Amount 5.000 Recovery = 100.40% J

Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.46 85 203157 11.84 ug/L 100 5) CHLOROMETHANE 4.93 50 204539 12.37 ug/L 98 6) VINYL CHLORIDE 5.13 62 145955 11.66 ug/L 99 7) BROMOMETHANE 6.03 94 135147 8.63 ug/L 99 8) CHLOROETHANE 6.17 64 120634 10.72 ug/L 98 9) TRICHLOROFLUOROMETHANE 6.71 101 337570 12.26 ug/L 99 10) ACETONE 7.64 43 33969 9.76 ug/L 100 11) 1,1-DICHLOROETHENE 7.98 61 380746 11.51 ug/L 97 12) METHYLENE CHLORIDE 8.95 49 377443 10.45 ug/L 97 13) METHYL TERT BUTYL ETHER 9.26 73 464520m 7.58 ug/L 14) TRANS-1,2-DICHLOROETHENE 9.60 61 408158 11.00 ug/L 99 -1-5-) - 1-, 1-DICHLOROETHANE l0.49 - 63 -- 515966 10.62 ug/L 99- 16) 2-BUTANONE (MEK) 11.30 43 64055 9.08 ug/L 91 17) 2,2-DICHLOROPROPANE 11.68 77 401127 10.99 ug/L 99 18) CIS-1,2-DICHLOROETHENE 11.76 96 279969 10.70 ug/L 92 19) CHLOROFORM 12.10 83 462159 10.65 ug/L 100 20) BROMOCHLOROMETHANE 12.48 49 234553 10.80 ug/L 96 21) 1,2-DICHLOROETHANE 13.81 62 281440 10.62 ug/L 100 24) 1,1,1-TRICHLOROETHANE 12.99 97 359639 10.52 ug/L 100 25) 1,1-DICHLOROPROPENE 13.33 75 386661 10.34 ug/L 99 26) CARBON TETRACHLORIDE 13.57 - 117 - --291331 11.08 ug/L 98 27) BENZENE - 13.93 78 1144405 9.78 ug/L 99 28) TRICHLOROETHENE 15.19 95 276912 10.08 ug/L 97 29) 1,2-DICHLOROPROPANE 15.53 63 314635 10.18 ug/L 98 3-0t DIBROMOMETHANE"_ _n- _. 16.18 174 80453 - 10:78-- ug/L 94 31) BROMODICHLOROMETHANE 16.02 83 314449 10.16 ug/L 100 32) 2-CHLOROETHYL VINYL ETHER 16.53 63 96068 10.96 ug/L 97 33) Methyl iso-butyl ketone 16.60 58 49558 10.52 ug/L 84 ------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration 1109C10.D HP110101.M Fri Nov 09 11:29:23 2001 Page 1

NYC-WTC 000000926

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