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VOC analysis results, sample AD26386, Nov 5 2001

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DEP laboratory report for sample AD26386 analyzing volatile organic compounds on November 5, 2001.

NYC-WTC_000000805–000000809

Folder label: “524 up to 11/7/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\01NOV2\1102R40.D Vial: 6 Acq On 2 Nov 2001 5:12 pm Operator: Sample : ref 40 Inst : GC/MS Ins Misc Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Nov 5 11:56 2001 Quant Results File: HP110101.RES

Quant Method : C:\HPCHEM\1\METHODS\HP11010l.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Fri Nov 02 15:17:46 2001 Response via : Initial Calibration DataAcq Meth : HP110101

Internal Standards R.T. Qlon Response Conc Units Dev(Min) ------------------------------------------------------------------------- 1) 1,4-DIFLUOROBENZENE 14.47 114 938305 5.00 ug/L 0.03 22) CHLOROBENZENE-D5 21.07 117 840563 5.00 ug/L 0.03 50) 1,4-DICHLOROBENZENE-D4 26.23 152 367562 5.00 ug/L 0.03

System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 13.69 65 249855 4.51 ug/L 0.03 Spiked Amount 5.000 Recovery = 90.200 3) 4-BROMOFLUOROBENZENE 23.64 174 277851 5.70 ug/L 0.03 Spiked Amount 5.000 Recovery = 114.00% 23) TOLUENE-D8 17.80 98 1236593 4.87 ug/L 0.05 Spiked Amount 5.000 Recovery = 97.400

Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.50 85 1106839 44.15 ug/L 99 5) CHLOROMETHANE 5.03 50 766534 31.73 ug/L 100 6) VINYL CHLORIDE 5.15 62 530623 29.03 ug/L 100 7) BROMOMETHANE 6.10 94 870957 38.07 ug/L 99 8) CHLOROETHANE 6.22 64 574774 34.97 ug/L 99 9) TRICHLOROFLUOROMETHANE 6.76 101 1712673 42.59 ug/L 99 10) ACETONE 7.69 43 159653 31.40 ug/L 98 11) 1,1-DICHLOROETHENE 8.05 61 1699413 35.16 ug/L 97 12) METHYLENE CHLORIDE 9.02 49 1790683 33.94 ug/L 96 13) METHYL TERT BUTYL ETHER 9.31 73 2492387m 27.85 ug/L 14) TRANS-1,2-DICHLOROETHENE 9.67 61 2040937 37.65 ug/L 95 15) 1,1-DICHLOROETHANE 10.55 63 2661690 37.51 ug/L 99 16) 2-BUTANONE (MEK) 11.37 43 270744 26.28 ug/L 99 17) 2,2-DICHLOROPROPANE 11.75 77 2132873 39.99 ug/L 99 18) CIS-1,2-DICHLOROETHENE 11.85 96 1542153 40.37 ug/L 97 19) CHLOROFORM 12.17 83 2458601 38.80 ug/L 99 20) BROMOCHLOROMETHANE 12.55 49 1104910 34.85 ug/L 91 21) 1,2-DICHLOROETHANE 13.88 62 1313535 33.95 ug/L 99 24) 1,1,1-TRICHLOROETHANE 13.06 97 2024301 40.48 ug/L 99 25) 1,1-DICHLOROPROPENE 13.38 75 2070192 37.87 ug/L 99 26) CARBON TETRACHLORIDE 13.64 117 1618660 42.09 ug/L 100 27) BENZENE 14.00 78 6224514 36.39 ug/L 100 28) TRICHLOROETHENE 15.24 95 1558928 38.82 ug/L 96 29) 1,2-DICHLOROPROPANE 15.60 63 1599878 35.39 ug/L 99 30) DIBROMOMETHANE 16.26 174 471538 43.21 ug/L 91 31) BROMODICHLOROMETHANE 16.11 83 1723173 38.08 ug/L 100 32) 2-CHLOROETHYL VINYL ETHER 16.60 63 489698 38.21 ug/L 98 33) Methyl iso-butyl ketone 16.67 58 247181 35.87 ug/L 91 ------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration 1102R40.D HP102901.M Tue Nov 13 11:46:29 2001 Page 1

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NYC-WTC_000000807Source: NYC Law Department, mirrored locally

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