NYC-WTC_000232104

NYC 9/11 Public Portal Document

EMSL Analytical, Inc. 107 Haddon Ave., Westmont, NJ 08108 EMSL OrderID:040305286 Attn; Andrew/ M.N. Khan Customer ID; JLCC50 JLC Environmental Consultants, Inc. Customer PO: 200 Park Ave South, Suite 1001 Date Received: 04/05/03 12:23 AM New York, NY 10003 Fax: 212-420-6092 EMSL Order: 040305286 Project: #03-2744/NYCDEP—114 Liberty ST EMSL Project ID: Report Date: 04/14/03 Date Analyzed: 04/14/03

Silica, Crystalline Analysis Performed X-Ray Diffraction (XRD) Modified MOSH Method 7500, Issue 3,1/15/98

I Respirable Dust Airborne Silica I Sample Sample Silica Silica % Analytical Sample ID Identification Particle Volume Weight Cone. Weight Cone, Silica Sensitivity ID (L) (mg) (mg/m^) (mg) (mg/m’) (riig/ii/)

MB13687;3QC lOTH FLR DINING Quartz 408 0.601 1.4730 0.0070 0.0172 1.2 0.0110 STANDARD 0r030Q Quartz N/A N/A N/A 0,025 N/A N/A N/A LAB BLANK Quartz 0 N/A N/A <0.0045 N/A N/A N/A

Notes:

1. Bulk sample not submitted with sample set. 2. Discernable fleld blank not submined with sample set. 3. Results are not field blank corrected.

Disclaimer: The laboratory can only verify the concentration of silica on the filter and not the final concentration due to data obtained by non-laboratory personnel. In the absence of a bulk dust sample, neither the specific forms of crystalline silica nor the interfering species can be fully determined. Hence, the amount for each phase, if anticipated, will be analyzed based on primary, secondary, and/or tertiary peak data with comparison to calibration curves of known standards. It should be noted that air samples are meant for only quantifying silica (or a mineral phase) which must first be identified from a bulk dust sample. “<” means less than the stated value. The lowest reportable value is equivalent to the Analytical Sensitivity that is calculated from the lowest reproducible amount of specific inineral delectable by the instrument.

Anant Samndra, Fh.D. Analyst Stephen Siegel, CI^Lah Manager Or other approved signatory

AIHA Accredited - Laboratory ID #100194 Page 3 of 3

CITY_DEP_WORBY_CANNATA_SUBP_000085295

NYC-WTC_000232106