NYC 9/11 Public Portal Document
Diun» 2. Post cleaning air samples for fibrous glass and silica shall be collected concurrently with the
asbestos clearance air sampling procedures specified herein. Five samples for fibrous glass and one
sample for silica shall be collected in each apartment.
3. Wipe samples shall be collected before and after cleaning for lead, dioxin, and PAHs.
Prior to the cleaning activities, three wipe samples shall be collected for each of these parameters in
each apartment. The sampling locations shall be a wall, a bare floor, and a counter or tabletop.
After cleaning activities, three wipe samples shall be collected for each of these parameters in each
apartment. The sampling locations shall be a wall, a bare floor, and a counter or tabletop; preferably
at the same location as the pre-cleaning samples.
4. The required sampling and analytical procedures are specified in Table 1.
Table 1: Sampling and Analytical Methods
Parameter Description Sampling Analytical Method Maximum
Methodology Turnaround
Time
Lead Wipe samples HUD Appendix 13.1 EPA Method SW-846-6010B 1 day
PAHs Wipe samples ASTM D6661-01 ASTM-6661-01 14 days
EPA SW-846-8270C
Dioxin Wipe samples ASTM 6661-01 ASTM 6661-01 14 days
EPA Method SW-846-8290
Fibrous Glass Air samples NIOSH 7400 NIOSH 7400, 3 days
Counting Method “B”
Crystalline Air samples NIOSH 7500 NIOSH 7500 (XRD) 14 days
Silica
5. The detection limit for PAHs shall be no greater than 2.5(xg/m2.
6. Samples containing concentrations of specific congeneric analytes (PCDDs and PCDFs) considered
within the scope of the dioxin sampling method that are greater than ten times the upper MCLs must
be analyzed by a protocol designed for such concentration levels, e.g. Method 8280. Analytical
results shall be reported using a 2,3,7,8-TCDD toxicity equivalency factor (TEF). All non-detect
congeners shall be reported at 50% of the analytical sensitivity, thereby yielding a recalculated TEF.
Asbestos Air Sample Collection and Analysis
I. All asbestos air sampling methodologies shall be in accordance with the applicable sections of Title
15, Chapter 1 of the Rules of the City of New York and AHERA.
2. Asbestos clearance air samples shall be analyzed in accordance with the NIOSH 7400 Method, and
analyzed by PCM followed by TEM. The laboratory shall report a PCMe value of all fibers greater
than 5 microns in length. Therefore, the lab shall report PCM, TEM and PCMe values for each
sample. The detection limit shall be 0.0004 f/cc.
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