' ATC ASSOCIATES INC. - TEM ANALYSIS
LAB GROUP it- 5759 - 17'25 01
(
Lab Sample No 62530 Filter Type MCE 25 mm Operator - ~,
Client Spl. No. 24 Filter Area 355 mm"2
II
Instrument I.D EM 10 CP.X Grid I.D. Disk No.
Screen Magnification 16,400X '.GO: Area 2.01124 mm'_
Acc. Voltage 80 kV No. GO to be Analyzed 4.72. Struct. Corsod. to 70 s -mm
I GO.
No Coord.
Structure
No.
Structure Type
>0.5 um
Length I.D. of Structure EDS
N or,/
(Nonasb.
F B C M < 5 um >. 5urn Chrys. Amphibole Nonasb. Ambig./ND Elements)
J -k~ —.—
I
I
I
Li
I
I
Photo No. (from 1 in 5 asbestos- Identify all structures using EDS Check diffraction for asbestos Store all unrepealed spectra
conta ini ng samples) I.GrIl acceptance: structures u to 70e r11tn (let 4)
I <10% undlasolve t r, over or o e
Struct. = > 0.5um & > 5:1 Aspect Ratio
<I0% particulate coverage >50% coverage Totals
Na Not Observed (EDS spectrum or diffraction pattern) t least 20 unfolded or overlapped grid squares
<5% holes or opaque areas
Positive diffraction pattern properties conforming
to laboratory identification criteria observed. Unused portion
Par ahry.otila: 0.77nm .pacing roc (020) reflections. of cuter Chrysotile
0.57nm spacing [or the layer line repeat, . .kin. Avoided portion
of (110) and (130) reflections. of filter
Per amphiboles: 0.53nm Layer line repeat, and appre[. Portion of filter (2mm wide)
3.5 ratio of son-twinned layer line spot .pacing to .object la
vaammation
I Amphibole
layer line repeat distance (0.53nm).
EDS spectrum conforming to laboratory r AMPHIBOLES ~ Ambiguous
identification criteria observed.
P= Single Fiber (1-3 Intersections = 1-3 flbcra) j AIIloslte
B= Bundle (>3 fibers <1 fiber diameter apart) 25mm filter i Crocidolite Non —asbestos
C= Cluster (>7 Intersections) (—stopping Buln: Anth°phylhte
M- Matrix
oS a/e.o. or In fat 4 Trernolite
NSD= No Structures Detected Non —Identified
Actinolite
L\DATA\PmVATE\ wiKSc\cADDV'EM7 9/22/08
NYC-WTC 000104291
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NYC-WTC_000104291Source: NYC Law Department, mirrored locally