NYC 9/11 Public Portal Document
I ATC ASSOCIATES INC. - TEM ANALYSIS
I Lab Sample Nc.
Client Spl. NO
62565
H-11
LAB GROUP 4.
Filter
5"70 - 10'2
Type MCE 1 5 mm
Filter Area 385 mm-2
31
Operstc
I Insnrumenc 1. D EM 10 CPX Grid 0.0. Cask Nc
Screen Magnification i6.400X !GOI Area 0.01134 mm Comments
Acc. Voltage 80 kV No. GO to be Analyzed 4.731 Struc~ rand Ic 2simm'_
GO. Structure structure Type Length I.D. of Structure N or l/ EDS
Lii %0.5 um , (Nonasb.
No Coord. No. F B C M Sum Chrys. Amphibole Nonasb. Ambig./ND Elements
< 5 um
~
J I
— l
— c—
— e,
G -
El
I
t
l
1
I
I i i I i i
Photo No. (from I in 5 asbestos- Identify all atructures using EDS Check diffraction for asbestos Store all unrepeated spectra J
containing samples) Grid accaptance: structures up to 70s cltm (lot 4)
<50% undlesolve 1 er. overappe or o e
I Struct = > 0.5um & > 5:1 Aspect Ratio
<I0% particulate coverage >50% coverage Totals
N= Not Observed (EDS spectrum or diffraction pattern) at least 20 unfolded or overlapped grid squares
<5% holes or opaque areas
Positive diffraction pattern properties conforming
to Laboratory identification criteria observed. Unused portion
For ahrysatilr. 0.73nm apaeing for (020) reflections. of filter Chrysotile
0.53am apamng for the layer line repeal streakcing Avoided portion
of (110) and (170) reflections. of filter
For amphiboles: 0.53nm layer line repeat and approa. ( Portion of filter (2mm side)
3.5 ratio of non-tetnned layer line spat spacing to I aubJeet In
exammatioo
Amphibole
layer line repeat distance (O.53nm). \
1 EDS spectrum conforming to laboratory
Identification criteria observed.
F= Single Fiber (1-3 intersections = 1-3 fibers)
8= Bundle (>7 fibers <1 fiber diameter apart) 25mm filter
AMPHIBOLES
Amosite
Croeidalite
Ambiguous
Non —asbestos
C= Cluster (>3 Intersection.)
rat= Matrix Stopping Aule,: A R th o P h .1' Mite
NSD= No Structures Detected I >50 0/0.0. or in lit 4 C.O. Tremolite
Actinolite Nan —Identified
I L\DATA\PRIVATE\M1KEG\CAD0~1'EM3 9/22/99
NYC-WTC 000104345
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