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← Document results/DEP Box 68/508 X 1/7/02 A 1/10-1/11/02
Document / 7 pages

Pesticide method validation data, Jan 2002

Machine-extracted title · confidence 100%

Technical report displaying calibration data and surrogate recovery results for pesticide analysis methods in early 2002.

NYC-WTC_000089845–000089851

Folder label: “508 X 1/7/02 A 1/10-1/11/02

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Scanned page image, NYC-WTC_000089845
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Response Factor Report Instrumen

Method : C:\MSDCHEM\1\METHODS\020110T.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides - Toxaphene Last Update : Fri Jan 11 08:14:26 2002

Calibration Files 1 =TOXC1.D 2 =T0XC2.D 3 =T0XC3.D

Compound 1 2 3 Avg %RSD

1) Toxaphene Peak 1 3.741 4.068 4.157 3.989 E7 5.49 2) Toxaphene Peak 2 7.571 7.731 7.597 7.633 E7 1.12 3) Toxaphene Peak 3 3.499 3.695 3.630 3.608 E7 2.77 4) Toxaphene Peak 4 1.558 1.648 1.611 1.605 E8 2.83 5) Toxaphene Peak 5 5.609 6.398 6.457 6.155 E7 7.70 6) S 2,4-ODD SURROGATE 3.411 3.195 3.271 3.292 E9 3.32

Signal #2 Calibration Files 1 =TOXC1.D 2 =T0XC2.D 3 =TOXC3.D

Compound 1 2 3 Avg %RSD

1) Toxaphene Peak 1 2.299 2.330 2.309 2.313 E7 0.68 2) Toxaphene Peak 2 1.075 1.144 1.170 1.129 E8 4.36 3) Toxaphene Peak 3 3.928 3.822 3.917 3.889 E7 1.50 4) Toxaphene Peak 4 1.020 1.091 1.110 ■ 1.074 E8 4.42 5) Toxaphene Peak 5 1.200 1.346 1.332 1.293 E8 6.23 6) S 2,4-ODD SURROGATE 2.710 2.297 2.343 2.450 E9 9.24

(#) = Out of Range 020110T.M Fri Jan 11 11:05:52 2002 Page 1

NYC-WTC_000089845

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NYC-WTC_000089845Source: NYC Law Department, mirrored locally

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