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Toxaphene analysis results for samples TOXC1-3, Dec 2001

Machine-extracted title · confidence 90%

Chemical analysis report listing toxaphene compound concentrations and surrogate recovery metrics from December 2001.

NYC-WTC_000089559–000089567

Folder label: “508 X 11/27/01 A 12/4-12/26/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\1\DATA\508\011224B\TOXUR.D\ECD1A.CH Vial: 9 Signal #2 : C:\MSDCHEM\1\DATA\508\011224B\TOXUR.D\ECD2B.CH Acq On : 24 Dec 2001 4:31 pm Operator: Nefliu Sample : tox uextracted ref Inst : Instrume Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Dec 31 15:19:49 2001 Quant Results File: 011224T.RES

Quant Method : C:\MSDCHEM\1\METHODS\011224T.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides - Toxaphene Last Update : Wed Dec 26 10:40:08 2001 Response via : Initial Calibration DataAcq Meth : MDL508.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 Conc#l Conc#2

System Monitoring Compounds 6) S 2,4-DDD SURROGAT 14.35 14.98 789.5E6 449.6E6 0.197m 0.170m Spiked Amount 0.200 Recovery 98.50% 85.00% Target Compounds 1) Toxaphene Peak 1 14.76 15.73 256.5E6 46030224 5.406m 2.026m# 2) Toxaphene Peak 2 15.15 16.13 261.9E6 534.0E6 3.102m 4.806m# 3) Toxaphene Peak 3 15.54 16.29 453.5E6 100.9E6 9.372m 2.687m# 4) Toxaphene Peak 4 17.19 16.71 473.0E6 374.4E6 2.491m 3.468m# 5) Toxaphene Peak 5 17.56 17.79 56837829 301.9E6 0.743m 2.414m#

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. TOXUR.D 011224T.M Mon Dec 31 15:22:03 2001 Page 1

NYC-WTC_000089566

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NYC-WTC_000089566Source: NYC Law Department, mirrored locally

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