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Chlordane analysis calibration data, December 2001

Machine-extracted title · confidence 90%

Calibration data and compound recovery statistics for chlordane analysis conducted in December 2001.

NYC-WTC_000055941–000055947

Folder label: “508 X 11/16/01 A 12/14/01 - 12/16/01

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Scanned page image, NYC-WTC_000055946
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\1\DATA\508\011214C\TOXUR.D\ECD1A.CH Vial: 12 Signal #2 : C:\MSDCHEM\1\DATA\508\011214C\TOXUR.D\ECD2B.CH Acq On : 14 Dec 2001 7:35 pm Operator: Nefliu Sample : tox unextracted ref Inst : Instrumen Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Jan 03 10:36:21 2002 Quant Results File: 011214T.RES

Quant Method : C:\MSDCHEM\1\METHODS\011214T.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides - Toxaphene Last Update : Mon Dec 17 14:19:26 2001 Response via : Initial Calibration DataAcq Meth : MDL508.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 Conc#l Cone#2

System Monitoring Compounds 6) s 2,4-DDD SURROGAT 14.33 14.97 751.2E6 533.4E6 0.205m 0.183m Spiked Amount 0.200 Recovery = 102.50% 91.50%

Target Compounds 1) Toxaphene Peak 1 14.75 15.72 218.5E6 48792683 4.009m 2.066m# 2) Toxaphene Peak 2 15.14 16.13 226.3E6 548.8E6 3.108m 4.627m# 3) Toxaphene Peak 3 15.52 16.28 408.3E6 104.6E6 10.068m 2.749m# 4) Toxaphene Peak 4 17.17 16.70 445.OE6 389.OE6 2.612m 3.613m# 5) Toxaphene Peak 5 17.55 17.78 98652766 313.3E6 1.402m 2.395m#

(wos—

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. TOXUR.D 011214T.M Thu Jan 03 10:37:54 2002 Page 1

NYC-WTC_000055946

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NYC-WTC_000055946Source: NYC Law Department, mirrored locally

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