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GC/MS analysis results for sample AD23838, Nov 2 2001

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Laboratory report documenting GC/MS analysis of sample AD23838 conducted on November 2, 2001, identifying unknown compounds.

NYC-WTC_000089346–000089365

Folder label: “GC/MS Scan 10/1/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\OCT3001\23838.D Vial: 12 Acq On : 31 Oct 2001 1:15 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.309 133 138 144 rBV 37965 79307 1.06% 0.212% 2 6.419 146 150 161 rVV2 61593 163345 2.18% 0.436% 3 6.547 161 164 173 rW 31246 78229 1.04% 0.209% 4 6.667 173 177 187 rVB 40456 91122 1.22% 0.243% 5 7.686 284 288 294 rBV 84041 197563 2 . '63% 0.528%

6 11.578 705 712 721 rBV 58757 147163 1.96% 0.393% 7 11.716 721 727 749 rBV 2099814 5287746 70.53% 14.125% 8 15.324 1113 1120 1138 rBV 3374214 7194656 95.96% 19.219% .9 20.602 1688 1695 1715 rBV 3381322 7497679 100.00% 20.029% 10 25.027 2170 2177 2188 rBV 3108203 6672639 89.00% 17.825%

11 29.452 2654 2659 2665 rBV 71383 137271 1.83% 0.367% 12 31.591 2887 2892 2897 rBV 53431 109102 1.46% 0.291% 13 31.683 2897 2902 2910 rVB 59109 121484 1.62% 0.325% 14 32.674 3005 3010 3019 rBV2 53041 112795 1.50% 0.301% 15 33.060 3044 3052 3068 rBV2 2161063 5157406 68.79% 13.777% 16 33.629 3107 3114 3123 rBV 56665 134484 1.79% 0.359% 17__ 34-..556 •3 211-3 215-3 22 4-rVB- -36686 —8-2-1-39 —1—10%- -0-219%- - 18 37.164 3490 3499 3516 rBV2 1471423 4170697 55.63% 11.141%

Sum of corrected areas: 37434827

_23838_.D__NP103001.M ____ Thu_Nov_01. 14 :33 :22_2001-

NYC-WTC_000089351

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NYC-WTC_000089351Source: NYC Law Department, mirrored locally

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