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GC/MS analysis results for sample AD23839, Nov 1 2001

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Laboratory report documenting GC/MS analysis of sample AD23839 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089366–000089384

Folder label: “GC/MS Scan 10/1/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\OCT3001\238.39.D Vial: 13 Acq On : 31 Oct 2001 2:14 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.428 147 151 161 rW2 51307 124456 1.72% 0.343% 2 7.695 286 289 302 rBV 53677 144202 2.00% 0.397% 3 11.569 705 711 721 rBV 59323 144313 2.00% 0.398% 4 11.716 721 727 746 rW 2064616 5165664 71.55% 14.229% 5 15.324 1113 1120 1137 rBV 3225392 7037599 97.47% 19.385% 6 20.602 1688 1695 1712 rBV 3326722 7219922 100.00% 19.887% 7 25.027 2170 2177 2189 rBV 2967093 6370160 88.23% 17.546% 8 29.452 2654 2659 2667 rBV 152359 291219 4.03% 0.802% 9 30.646 2784 2789 2795 rBV 41398 82153 1.14% 0.226% 10 31.591 2884 2892 2898 rBV 111157 224590 3.11% 0.619% 11 31.683 2898 2902 2912 rVB 87817 178368 2.47% 0.491% 12 32.674 3003 3010 3019 rBV 73383 164261 2.28% 0.452% 13 33.060 3044 3052 3066 rBV2 2029873 4798893 66.47% 13.218% 14 33.638 3110 3115 3124 rBV 80929 185301 2.57% 0.510% 15 34.556 3210 3215 3228 rVB 56463 129695 1.80% 0.357% 16 35.447 3306 3312 3325 rBV2 39882 110329 1.53% 0.304% . 17 _3-7-.-164—349 0-34 9 9-3 523-r-BV2 -1-372 6 68—3 93-3-742—54~4 8 %— 10.835%

Sum of corrected areas: 36304867 23839.D NP103001.M Thu Nov 01 14:35:44 2001

NYC-WTC_000089371

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NYC-WTC_000089371Source: NYC Law Department, mirrored locally

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