GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
NYC-WTC_000089278–000089298Folder label: “GC/MS Scan 10/1/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\OCT3001\LB.D Vial: 8 Acq On : 30 Oct 2001 9:22 pm Operator:.209 GALOS Sample : lab blk 10/1 / J' Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 1 10:18 2001 Quant Results File: NP101901.RES Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrat0t) . , Title. : 209 625/TCLP calibration table f) Last Update : Tue Oct 23 10:12:13 2001 v Response via : Initial Calibration YV* V\ r DataAcq Meth : NP101901 '
Internal Standards R.T. Qlon .Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.71 152 1018809 20.00 ug/1 -0.05 19)' Naphthalene-d8 15.32 136 4082536 20.00 ug/1 -0.05 31) Acenaphthene-dlO 20.60 164 .1994589 20.00 ug/1 -0.03 49) Phenanthrene-dlO 25.03 188 .2868194m 20.00 ug/1 -0.03 59) Chrysene-dl2 33.06 240 1703254 20.00 ug/1 -0.04 68) Perylene-dl2 37.17 264 1166671 20.00 ug/1 -0.03 System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 11.71 132 704 0.01 ug/1 0.45 Spiked Amount 75.000 Recovery = 0.01% 7) 1,2-Dichlorobenzene-d4 12.23 152 12153 0.17 ug/1 -0.04 Spiked Amount 50.000 Recovery = 0.34% 20) Nitrobenzene-d5 0.00 82 . 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.74 172 4618 0.02 ug/1 0.09 Spiked Amount 50.000 Recovery = 0.04% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery 0.00% 62)- Terphenyl-dl4 29.92 244 ■ 123 0.00 ug/1 -0.06 Spiked Amount 50.000 Recovery '= 0.00% Target Compounds Qvalue ' 2) Pyridine 5.26 79- 210 N.D. 3) N-nitroso-dimethyl amine 5.17 74 . •. 765 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. -- 10)-2-Chlorophenol--- —. — -0.00- 128- --- 0— NtD-. 11) 1,3-Dichlorobenzene. 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146. 0- N.D. --7-=—13 -) - -1-7-2 - D ichl- o r ob en z ene-- -0^00 T46-’ NtDT '■^^T4)“2-'Methylph'eriol“~~‘~‘‘‘‘^ “OTO'O— '0 N.D. 15) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol ___ 0.00 108 0 N.D. --- 17') ~N-Nitroso - di“n-propylamineTT—0-00-- 70—- N7D7 18) Hexachloroethane 0.00 117 ' 0 N.D. 21) Nitrobenzene 0.00 77; / . 0 N.D. 22) Isophorone 0.00 82 0 N.D. (#) = qualifier out of range (m) = manual integration LB.D NP103001.M Mon Nov 05 08:53:59 2001 Page 1
NYC-WTC_000089278
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NYC-WTC_000088184
Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088700
Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087496
Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087980
Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089311
Laboratory report documenting GC/MS analysis of sample AD23799 conducted on November 1, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089030
GC/MS analysis report with TCLP calibration table data from October 16, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086768
Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086788
Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087132
Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086624
Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089476
Laboratory report documenting GC/MS analysis of sample AD23834 conducted on November 1, 2001, identifying unknown compounds.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069154
Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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NYC-WTC_000089273
Gas chromatography-mass spectrometry scan results recorded on October 1, 2001 for environmental samples.
Filed in the same folder
NYC-WTC_000089274
Detailed GC/MS calibration report for October 1, 2001, including peak data and method parameters.
Filed in the same folder
NYC-WTC_000089299
Laboratory record for sample AD23798 showing detection of unknown compounds on November 1, 2001.
Filed in the same folder
NYC-WTC_000089311
Laboratory report documenting GC/MS analysis of sample AD23799 conducted on November 1, 2001, identifying unknown compounds.
Filed in the same folder
NYC-WTC_000089333
Laboratory report documenting GC/MS analysis of sample AD23837 conducted on November 1, 2001, identifying unknown compounds.
Filed in the same folder