NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\OCT1501\23721.D Vial: 17
Acq On : 16 Oct 2001 3:49 am Operator: 209 GALOS
Sample : gc/ms unknown Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator)
Title : 209 625/TCLP calibration table 7/16/01
Library : C:\DATABASE\NBS75K.L
Peak Number 3 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
7.76 ,1.2 9 ug/1 120056 1,4-Dichlorobenzene-d4 11.77
Hit# of 5 Te: tive ID MW MolForm CAS# Qual
1 2-Pentano: , 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 53
2 Acetic id, 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 28
3 CH2=CHCH2C(O)OCH3 100 C5H8O2 003724-55-8 10
4 Moj^oline, 4-methyl- _________ 101 C5H11NO . 000109-02-4 9
Abundance Scan 296 (7.755 min): 23721 .D (-) m/ z 42.95 100.00%
4)3
59
5000-
101 I ' I I r-i , I I , , , I . , , , I ,
TlZz->
—r-r-r-r-p-r-n-r-p—r-i-r-f-r ■t-r
10 20 30
3^ Il
40 50 60
83
' I ' ' ' ' I ' ' ' ' I '
70 80 90
4
100 tIO
7.40 7.60
59.05
7.80 8.00
50.79%
Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl-
4)3
5000
59 ■ '7.40' '7.6O 8.00
m/z 101.05 18.96%
27 101
.................. I I ..-79, J, 83
rT+ ‘ I ' ' ' ' I '''
Tife-> 10 20 30 40 50 60 70 80 90 ’ 100 110
Abundance #3292: Acetic acid, 1,1 -dimethylethyl ester
' 4)3
-'-I . I /. I
7.40 7.60 7.80 8.00
5000 57 m/^ 58.05 15.15%
nfe->
\bundance
5000
10
15-
20
-27 -
30 40 50
' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' .' ‘ ' I ' ' ' ' I ' '
60 70
#1448; CH2=CHCH2C(O)OCH3
—4I3-——----- ■-
80 90
101
100
.I
110
-^7.40
m/z
i7.60—7.80 - '8.00 -
41.00 9.02%
.....................................38 I, I ' ' I ' '
I ‘ ' I ' ' ' ' I ' ' ' ' I*
T I . . , . I 7I , , . , , , , , I ■ , , ,^90I . , I
' ' I '' ' ' I '' ' ' I ' ' ' ' I' ''' I '
■nZz-> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00
23721.D NP091101.M Tue Oct 16 15:16:56 2001 Page 3
NYC-WTC_000089244
OCR can misread numbers and units. Confirm readings against the page image before using them.