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GC/MS analysis report, sample AD23721, Oct 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23721 showing detection of unknown compounds on October 17, 2001.

NYC-WTC_000089234–000089246

Folder label: “GC/MS Scan 9/28/01

Page image
Scanned page image, NYC-WTC_000089244
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\23721.D Vial: 17 Acq On : 16 Oct 2001 3:49 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L

Peak Number 3 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.76 ,1.2 9 ug/1 120056 1,4-Dichlorobenzene-d4 11.77

Hit# of 5 Te: tive ID MW MolForm CAS# Qual

1 2-Pentano: , 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 53 2 Acetic id, 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 28 3 CH2=CHCH2C(O)OCH3 100 C5H8O2 003724-55-8 10 4 Moj^oline, 4-methyl- _________ 101 C5H11NO . 000109-02-4 9 Abundance Scan 296 (7.755 min): 23721 .D (-) m/ z 42.95 100.00% 4)3

59 5000-

101 I ' I I r-i , I I , , , I . , , , I ,

TlZz-> —r-r-r-r-p-r-n-r-p—r-i-r-f-r ■t-r 10 20 30 3^ Il 40 50 60 83 ' I ' ' ' ' I ' ' ' ' I ' 70 80 90 4 100 tIO 7.40 7.60 59.05 7.80 8.00 50.79% Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 4)3

5000 59 ■ '7.40' '7.6O 8.00 m/z 101.05 18.96% 27 101 .................. I I ..-79, J, 83 rT+ ‘ I ' ' ' ' I ''' Tife-> 10 20 30 40 50 60 70 80 90 ’ 100 110 Abundance #3292: Acetic acid, 1,1 -dimethylethyl ester ' 4)3 -'-I . I /. I 7.40 7.60 7.80 8.00 5000 57 m/^ 58.05 15.15%

nfe-> \bundance

5000 10 15- 20 -27 - 30 40 50 ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' .' ‘ ' I ' ' ' ' I ' ' 60 70 #1448; CH2=CHCH2C(O)OCH3 —4I3-——----- ■- 80 90 101

100 .I 110

-^7.40 m/z i7.60—7.80 - '8.00 - 41.00 9.02%

.....................................38 I, I ' ' I ' ' I ‘ ' I ' ' ' ' I ' ' ' ' I* T I . . , . I 7I , , . , , , , , I ■ , , ,^90I . , I ' ' I '' ' ' I '' ' ' I ' ' ' ' I' ''' I ' ■nZz-> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00

23721.D NP091101.M Tue Oct 16 15:16:56 2001 Page 3

NYC-WTC_000089244

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NYC-WTC_000089244Source: NYC Law Department, mirrored locally

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