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GC/MS analysis results for sample AD23500, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23500 conducted on October 19, 2001.

NYC-WTC_000088826–000088852

Folder label: “GC/MS Scan 9/27/01

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NYC 9/11 Public Portal Document

Librar_y_Search_Compound Report

Data File ; C;\HPCHEM\1\DATA\OCT1601\23500.D Vial: 8 Acq On : 16 Oct 2001 9:05 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 17 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 15 R.T. EstConc Area Relative to ISTD R.T. 44.18 0.50 ug/1 41542 Perylene-dl2 37.23

Hit# of 5 intative ID MW MolForm CAS# Qua!

1 3,6-Dioxa22,4,5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 38 2 Trisilox^e, 1,1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 17 3 Tris (trzfmethylsilyl) borate 278 C9H27BO3Si3 004325-85-3 12 4 TrisiX’xane, octamethyl- 236 C8H24O2Si3 000107-51-7 12 Abundance Scan 4263 (44.178 min); 23500.D (-) m/z73700 100.00% 73 147 221

5000 281 355

UU ....... ....Tl.. 41 96 ........... "I" "I"" I I......... .. T m/z 147.00 111. < I. I. rpr., I,, ,, I 43 80 44.00 44.20 44.40 44.60 87717%

2.. ttZz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #41682: 3.6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4.4,5.5,7,7- 147 2:1

73 5000 43.80 44.00 44.20 44.40 44.60 191 ra/z 220.95 83.57% 117 rp-TTTp-njp/rrpk-ry^^ I_______ '" 'If" " I" " I" " r "' I" " I"'' I''" I" " I ■n/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet‘ * 73 147

281 43 80 44.00 44.20 44.40 44.60 5000 m/z“281.00 39.55%

369 ....................... ,................ 249 338 1 -rp-i-TTpnTTyrTTTp-YTTp-T-rTY^ 11 I ... I, , ,, I , A , I,,,. 11 ... I ... , I 40 60 80 1 00120140160180200220 240260280300 320340360380400 420 .... ■n/z-> Abundance #39028: Tris(trimethylsilyl)borate___ 7b 221 -43,80 44.00 44.20 44.40 44.60 m/z 354.95 35.74% 5000- 263

■n/z-> ... ............ 1.............. 40 60 80 1001201401601802002202^ 2602803(^320340360 ^0400420 ' 43.80 44.00 44.20 44.40 44.60

23500.D NP091101.M Thu Oct 18 10:18:17 2001 Page 17 1 NYC-WTC_'000088849

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NYC-WTC_000088849Source: NYC Law Department, mirrored locally

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