NYC 9/11 Public Portal Document
Librar_y_Search_Compound Report
Data File ; C;\HPCHEM\1\DATA\OCT1601\23500.D Vial: 8
Acq On : 16 Oct 2001 9:05 pm Operator: 209 GALOS
Sample : gc/ms unknown Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator)
Title : 209 625/TCLP calibration table 7/16/01
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 17 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 15
R.T. EstConc Area Relative to ISTD R.T.
44.18 0.50 ug/1 41542 Perylene-dl2 37.23
Hit# of 5 intative ID MW MolForm CAS# Qua!
1 3,6-Dioxa22,4,5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 38
2 Trisilox^e, 1,1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 17
3 Tris (trzfmethylsilyl) borate 278 C9H27BO3Si3 004325-85-3 12
4 TrisiX’xane, octamethyl- 236 C8H24O2Si3 000107-51-7 12
Abundance Scan 4263 (44.178 min); 23500.D (-) m/z73700 100.00%
73 147 221
5000
281 355
UU ....... ....Tl..
41
96 ...........
"I" "I""
I I......... .. T m/z 147.00
111. < I. I. rpr., I,, ,, I
43 80 44.00 44.20 44.40 44.60
87717%
2..
ttZz-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #41682: 3.6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4.4,5.5,7,7-
147 2:1
73
5000
43.80 44.00 44.20 44.40 44.60
191 ra/z 220.95 83.57%
117
rp-TTTp-njp/rrpk-ry^^
I_______ '" 'If" " I" " I" " r "' I" " I"'' I''" I" " I
■n/z-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet‘ *
73 147
281 43 80 44.00 44.20 44.40 44.60
5000 m/z“281.00 39.55%
369
....................... ,................ 249 338 1
-rp-i-TTpnTTyrTTTp-YTTp-T-rTY^ 11 I ... I, , ,, I , A , I,,,. 11 ... I ... , I
40 60 80 1 00120140160180200220 240260280300 320340360380400 420
....
■n/z->
Abundance #39028: Tris(trimethylsilyl)borate___
7b 221 -43,80 44.00 44.20 44.40 44.60
m/z 354.95 35.74%
5000-
263
■n/z->
... ............ 1..............
40 60 80 1001201401601802002202^ 2602803(^320340360 ^0400420 ' 43.80 44.00 44.20 44.40 44.60
23500.D NP091101.M Thu Oct 18 10:18:17 2001 Page 17
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NYC-WTC_'000088849
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