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GC/MS analysis results for sample AD23324, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.

NYC-WTC_000088316–000088345

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088335
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\0CT12 01\23324.D vial: 17 Acq On : 12 Oct 2001 5:46 pm Operator: 2 09 GTkLOS Sample : gc/ms unknown Inst : GC/MS 209 Mise • Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : .C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Heneicosane Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 32.73 6.56 ug/1 744356 Chrysene-dl2 33.12 Hit# Of 5 Tentative ID MW . MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 91 2 Eicosane 282 C20H42 000112-95-8 91 3 Octadecane 254 C18H38 000593-45-3 91 4 Tetracosane ____________________338 C24H50 000646-31-1 90' Sundance Scan 3016 (32.726 min): 23324.D (-) m/z 57.00 100.00% e:

85 5000 4

J 141 169 197 225 253 281 T-r-p-r-n-f Hr 32.40 32.60 32.80 33.00 352 ■i‘‘\'rTyTT7^ryriTTYinn-tYrn-riTrTT^^ I ’ ‘' I " '' I' ‘' I m/z 71.00 71.54% TTfe-> Abundance 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #42201; Heneicosane fl 57

5000 85 n 32.40 32.60 32.80 33.00 ' I ' ' ' ' I

m/z 43.05 67733% 268 296 TT+pn*‘tTyTrTTYrTTTp-VT^^ ' r ''' r ''' I'''' I'''' I'''' I'''' I'''' I' '' I'''' I p/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ^bundance #39862: Eicosane 57

T 32.40 32.60 32.80 33.00 5000 85 m/z 85.05 50.46%

i I J T , , 196 240 282 n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71561: Octadecane 57 32.40 32.60 32.80 33.00 m/z 41.05 26.60% 85 5000

224 254 I '''' I *' *' I ' I'' " I ’ ‘' I'''' I'''' I " •' I ’ ‘' I' ‘' I . ........ , A , Tl/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 32.40 32.60 32.80 33.00

23324.D NP091101.M Mon Oct 15 10:33:48 2001 Page 13

NYC-WTC_000088335

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NYC-WTC_000088335Source: NYC Law Department, mirrored locally

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