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GC/MS analysis results for sample AD23259, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23259 conducted on October 12, 2001.

NYC-WTC_000088069–000088078

Folder label: “GC/MS Scan 9/24/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0901\23259.D Vial: 5 Acq On 9 Oct 2001 5:16 pm Operator: 209 GALOS Sample g c/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,4-Dichlorobenzene-d4 Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 11.62 0.56 ug/1 111240 1,4-Dichlorobenzene-d4 11.77 Hit# Of 5 Tentative id MW MolForro CAS# Qual

1 l,4-Dichlpfobenzene-d4 150 C6C12D4 003855-82-1 50 2 Benzene-X 2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 12 3 4-Amino/-2-chlorobenzonitrile 152 C7H5C1N2 020925-27-3 9 4 IH-Py rolo[2,3-b]pyridine-2,6-dione 152 C7H8N2O2 017384-56-4 9 Abundance < Scan 717 (11.619 min): 23259.D (-) m/z 149.90 100.00% 1!i0

115 78 I I I I I I . I I I p . I I ' ' I I r-i— 52 40 ^3 11.20 11.40 11.60 11.8O''12.6F' ' I ' •" n " " 4^ m/z 151.90 . 66.19% Tife—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 ^bundance #9593:1,4-Dichlorobenzene-d4 1!i0

5000 115 78 11.20 11.40 11.60 11.80 12.00 52 m/z 114.90 35.60% 35 I i ' ' ' ' I ■n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5.6-dichloro- iSO —I I I I I I I p-l / ip-l I I I I I

115 11.20 11.40 11.60 11.80 12.00 5000 52 78 "mTz 78.05 20.19% fl 35 87 I I -nJiLp- 1 Wz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 ^bundance #10110: 4-Amino-2-chlorobenzonitrile I ' ' ' ' I ‘ ' 1!i2 11.20 11.40 11.60 11.80 12.00 Wz 52.00 14.84% 5000

90 117 125 76 ....... ' I ‘ ‘ I ' ‘ ' I ' ' ' ' I ' ' ' ' I ' ' ' ' 'n/z-> 30 40 50 60 70 I80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

23259.D NP091101.M Thu Oct 11 10:42:00 2001 Page 1

NYC-WTC_000088077

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NYC-WTC_000088077Source: NYC Law Department, mirrored locally

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