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GC/MS analysis results for sample AD23258, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23258 conducted on October 12, 2001.

NYC-WTC_000088048–000088068

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088055
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0901\23258 .D Vial; 4 Acq On 9 Oct 2001. 4:17 pm Operator: 209 GALOS Sample g c/ms unknown Inst ; GC/MS 209 Mise Multiplr; 1.00 MS Integration Params; LSCINT.P

Quant Method ; C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 6.50 0.43 ug/1 85219 1,4-Dichlorobenzene-d4 11.76 Hit# of' 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanrone 100 C6H12O 000591-78-6 91 2 Oxir^e, 2-methyl-2- (1-methylethyl) 100 C6H12O 072221-03-5 78 3 2-H^anone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 74 4 Met/iyl Isobutyl Ketone______________ 100 C6H12O 000108-10-1 58 ^bundanc/ Scan 159 (6.504 min): 23258.D (-) m/’z 42.95 100.00% 43 (1 58 5000

71 85 6.20 6.40 6.60 6.80 ' -......-..J: 50 I I I TT-p-rV-' I ' ' ' ' I ' ' '' I ' ''' 1 ' ................. ...................... m/z 58.05 59.44% Ti/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #1556: 2-Hexanone 43

58 5000 6.20 6.40 6.60 6.80 m/z 57.00 17.58% 27 71 85 100 , |i|........ I, ■ I I ■ ... I I ... I ■■■■ I ■ I " ......... . I ' I' ' ' ' I ' Tl/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #1530: Oxirane. 2-methyl-2-(1-methylethyl)- 43 58 6.20 6.40 6.60 6.80 253 m/z 41.05 15.41% 71

30 85 100 1,>.>.I,,..II 'i ’ ’ ' ' I ’ Tl/z-> 20 30 40 50 60 70 80 90 ipg 110 120 130 140 Abundance #11968: 2-Hexanone, 4-hydroxy-3-propyl- 43 6.20 6.40 6.60 6.80 m/z 100.05 11.25% 58 553 29

100 T-p-T ' 1 ' ' ' ' I I ' ' ' I ' ' J. 71 I 85 ......................... 140. ‘ I ' ' ' ' H ' 1^1 I ' I ' '■

iiZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 6.20 6.40 6.60 6.80

23258.D NP091101.M Thu Oct 11 10:40:58 2001 Page 1

NYC-WTC_000088055

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NYC-WTC_000088055Source: NYC Law Department, mirrored locally

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