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GC/MS calibration data sheet for October 5, 2001

Machine-extracted title · confidence 90%

Laboratory data sheet listing extraction dates and calibration results for deuterated standards.

NYC-WTC_000087980–000087999

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000087986
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\OCT0401\LB.D Vial: 9 Acq On 4 Oct 2001 11:22 pm Operator: 209 GALOS Sample 9/24 Inst : GC/MS 209 Mise •Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ★*★★★***★**★★**★*★★***★★*****★★*★**★★★****★***★****★★★★★*★**★*★★★**** i Peak Number 1 2-Hexanone Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

6.48 0.69 ug/1 100958 1,4-Dichlorobenzene-d4 11.78

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexajifbne 100 C6H12O 000591-78-6 86 2 2-He: none, 4-hydroxy-5-methyl-3-pr 172 C10H20O2 061141-74-0 83 3 Meth 1 Isobutyl Ketone 100 C6H12O 000108-10-1 58 4 2 rXexanone, 4 -methyl- 114 C7H14O 000105-42-0 39 *\bundance, Scan 157 (6.484 min): LB.D (-) m/z 42.95 100.00% 4)3

58 5000

71 85 100 __6:2O__64O__J,6O__6;8O^^ ■’’m' 11" ' I " " I " " I “ " I" " I" " I" " I ‘ 'I m/z 58.0,5 55.07% Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63385-. 2-Hexanone 4)3

5000 58 6.20 ' ' 6.40 6.60 6.80 29 m/z 41.0,5 13.96% I 39 71 85 100 ' I" " I ’ I h " " I ....... ............... ................ m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #15807; 2-Hex3iione. 4-hydroxy-5-rnethyl-3-propyl- 43 - —- -

6.20 6.40 6.60 6.80 5000 m/z 57,. 00 12.52% 58 27 I

fn/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105__ <^bundance #63354: Methyl Isobutyl Ketone 4)3 6.20 6.40 6.60 6.80 m/z 100.00 10.32% 5000 58

I' •" I J. 85 100 I' " ' I " " I ‘ ' I" " I " " I " " I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 \aaa 6.20 6.40 6.60 6.80

LB.D NP091101.M Tue Oct 09 12:49:38 2001 Page' 1

NYC-WTC_000087986

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NYC-WTC_000087986Source: NYC Law Department, mirrored locally

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GC/MS calibration table, Oct 1 2001 · Box DEP Box 67

NYC-WTC_000089278

GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996

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