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GC/MS analysis results for sample AD23080, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23080 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087817–000087841

Folder label: “GC/MS Scan 9/21/01

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Scanned page image, NYC-WTC_000087826
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NYC 9/11 Public Portal Document ■ , . Liinrary bearen compound Report

'Data File C:\HPCHEM\1\DATA\OCT0 3 01\23080.D Vial: 7 Acq On 3 Oct 2001 6:30 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

6.62 0.40 ug/1 50152 1,4-Dichlorobenzene-d4 11.78

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexan01 102 C6H14O 000623-37-0 83 2 4-Heptlnol 116 C7H16O 000589-55-9 12 3 Gu^^iidine 59 CH5N3 000113-00-8 9 4 IkPropanamine, 2-methyl- 73 C4H11N ___ 000078-81-9 9 Abundance Scan <72 (6.623 min): 23080.D (-) m/ Z 59.05 10’0.00%

jLL 55

5000- 73

41 44 84 6.20 6.40 6.60 6.80 7.00 "" I" ’' I"" I" ■' I"" I" ” I"' M ..... h"'"'' I" " I' I " 11" I' I" m/z 55.00 71.28% m/2-> 5_. IO 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #63531: 3-Hexanol

55

5000 73 6.20 6.40 6.60 6.80 7.00 43 m/ z 73.00 47.68% 39 ....... ^.^.1 ' r ‘' I'''' IT ' •' I'''' I ' * I''' i I' I ' I' ‘' I'' -rp-rTTp-rrrp-T n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #64376: 4-Heptanol 56 73 6.20 6.40 6.60 6.80 7.00 5000 43 m/z 4 0.95 24.58% 27 . 31 15 ; i 59 69 m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #100: Guanidine 43 59 6.20 6.40 ~ 6.60 6.80 7.00 m/z 43.05 22.09% 5000

17 27 31 +t P" hi/2~> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 6.20 6.40 6.60 6.80 7.00

23080.D NP091101.M Tue Oct 09 10:01:35 2001 Page 3

NYC-WTC_000087826

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NYC-WTC_000087826Source: NYC Law Department, mirrored locally

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