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GC/MS analysis results for sample AD22778, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22778 conducted on October 5, 2001, identifying unknown compounds.

NYC-WTC_000087682–000087693

Folder label: “GC/MS Scan 9/20/01

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Scanned page image, NYC-WTC_000087692
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0 201\22778.D Vial: 15 Acg On 3 Oct 2001 3:49 am Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 11.65 0.51 ug/1 60729 1,4-Dichlorobenzene-d4 11.79 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-D^hlorobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benz^amine, 2-methyl-4-nitro- 152 C7H8N2O2 000099-52-5 22 3 Berylenamine, 2-methyl-5-nitro- 152 C7H8N2O2 000099-55-8 22 4 Be/zene-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 17 ^bundande Scan 720 (11.648 min): 22778.D (-) m/z 149.85 100.00% 1!i0

ass 115 78 52 11.40 11.60 11.80 12.00 42 87 I ' ' I ' ' ' 'I ' ' m/z 151.90 , 62.06% -n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 1!i0

5000- 115 78 11.40 11.60 11.80 12.00 52 m/z 115.00 . 32.36% 87 ■Tife-> 30 35 40 50 ‘ I'''' I' 60 70 I ' '' ' r 80 90 100 110 120 I 130 140 414^ 150 160 Abundance #10129: Benzenamine, 2-methyl-4-nitro- 77 106 Ite

11.40 11.60 11.80 12.00 m7"z 78705 21.17% 5000 51 94 66 - I '' ' ' I ' '' ' I •n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #66885: Benzenamine, 2-methyl-5-nitro- 77 106 1!i2 11.40 11.60 11.80 12.00 m/z 52.00 . 14.88%

5000 51 94

T-r-p- ' 60 " ' 70 ' ' I ' ' ' ' I ' ' * ' I ' ' ' ' I ' ' ' ' I ■n/Z“> 30 40 50 80 90 100 110 120 130 140 150 160 11.40 11.60 11.80 12.00

22778.D NP091101.M Fri Oct 05 08:47:55 2001 Page 3 NYC-WTC_000087692

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NYC-WTC_000087692Source: NYC Law Department, mirrored locally

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