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GC/MS analysis results, sample AD22919, October 2001

Machine-extracted title · confidence 85%

Gas chromatography-mass spectrometry analysis of sample AD22919 conducted on October 5, 2001, identifying other unknown compounds.

NYC-WTC_000087623–000087643

Folder label: “GC/MS Scan 9/20/01

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NYC 9/11 Public Portal Document uxuidiy searcn compouna Report Data File : C;\HPCHEM\1\DATA\OCT0201\22919 .D Vial: 9 Acq On : 2 Oct 2001 9:56 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Hexatriacontane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 34.63 0.65 ug/1 82102 Chrysene-dl2 33.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Hexatriacontane 507 C36H74 000630-06-8 91. 2 Tetratetracontane 619 C44H90 007098-22-8 91) 3 Nonacosane 408 C29H60 000630-03-5 9(/ 4 Eicosane 282 C20H42 000112-95-8 87 Abundance Scan 3223 (34.632 min): 22919.D {-) m/z SYTOO 100.00% 57

85

34.40 34.60 34.80 35,00 Jjjj I127 J 155i 207 m/z 71.10 ■ 66.57% ■nZz-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #74636: Hexatriacontane c7

5000 85 34.40 34.60 34.80 35.00 m/z 43.0.0 67779% ■ . I . , , ................ .............................. I " ■ ■ I........................... I ■ ■ ■n/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #61068: Tetratetracontane 517

34.40 34.60 34.80 35.00 5000 m/z 85.05 43.43% 85

I fri^f‘*??9.1?7225 379407 590618 n-r-p Tl/Z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #54526: Nonacosane ■H" 43 34.40 34.60 34.80 35.00 m/z 55700 21.94% 71

TlZz-> ' ' I ' 50 ,+S 100 150 211239 200 250 300 379408 350 400 450 500 550 600 34.40 34.60 34.80 35.00

22919.D NP091101.M Thu Oct 04 10:03:40 2001 Page 9

NYC-WTC_000087638

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NYC-WTC_000087638Source: NYC Law Department, mirrored locally

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