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GC/MS analysis results for sample AD22914, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22914 conducted on October 5, 2001, noting other unknown compounds.

NYC-WTC_000087540–000087561

Folder label: “GC/MS Scan 9/20/01

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Scanned page image, NYC-WTC_000087547
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0201\22914.D Vial; 4 Acq On : 2 Oct 2001 5:03 pm Operator; 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 6.38 0.51 ug/1 62153 1,4-Dichlorobenzene-d4 11.79 Hit# Of .5 Tentative ID MW MolForm CAS# Qual

1 3 -H^anone 100 C6H12O 000589-38-8 86 2 3-pentanone, 2-methyl- 100 C6H12O 000565-69-5 47 3 Buxane, 2,2-dimethyl- 86 C6H14 000075-83-2 36 4 JIeptane, 3,3-dimethyl- 128 C9H20 004032-86-4 36 ^u/dance Scan 146 (6.381 min): 22914.D (-) m/z 43.05 100.00% 43 57

71 5000 100

6.00 6.20 6.40 6.60 6.80 TTrpTTTp-rrrpTTTpTTTpTTT^^ I +TrrTTjTrrrtr I* •' ‘I m/z 56795 84.02% n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Sundance #1528; 3-Hexanone 57

29 71 5000 6.00 6.20 6.40 6.60 6.^ 100 m/z 71.00 60.98%

I" " I' ‘ " I A |iin|nir|il TprrtTTTTTtr . ............. I' ........... I" " I" " I I "" ii/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 ^bundance #63398:3-Pentanone, 2-methyl- 5(7 43 __ 6.00 6 20 6,40 6.60 So 5000 m/z 100.05 31.95% 100 71

nfe-> Abundance i’"’I r "' I l|“-rTpn'i|l . ........... . 85 I" " I'" 'I" " I 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 #62861: Butane, 2,2-dimethyl- 43 57 71 l•"'l

6,00 “m/z 6.20 41.05 VI 6.40 6,60 21.05% 6,80

5000 29

15 ................ -tTyTTTTT r "' I'"' I"” I' r "' I tVz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.00 6.20 6.40 6.60 6.80

22914.D NP091101.M Wed Oct 03 09:48:52 2001 Page 1

NYC-WTC_000087547

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NYC-WTC_000087547Source: NYC Law Department, mirrored locally

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