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GC/MS analysis results for sample AD22913, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22913 conducted on October 5, 2001, noting other unknown compounds.

NYC-WTC_000087517–000087539

Folder label: “GC/MS Scan 9/20/01

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NYC 9/11 Public Portal Document rixuictxy ijearcn compouna Report

Data File ; C:\HPCHEM\1\DATA\OCT0201\22913.D Vial: 3 Acq On ; 2 Oct 2001 4:04 pm Operator; 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library ; C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Pentanol, 4-methyl- Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 6.73 0.41 ug/1 53136 1,4-Dichlorobenzene-d4 11.78 Hit# of 5/ Tentative ID MW MolForm CAS# Qual a »1 2-Pentanol, 4-methyl- 102 C6H14O 000108-11-2 83 2 2-Hexmol 102 C6H14O 000626-93-7 74 3 2-Hex4nol, (R)- 102 C6H14O 026549-24-6 64 4 2-He?canol, (S) - 102 C6H14O 052019-78-0 64 Abundance y Scan 184 (6.733 min): 22913. D (-) m/z 44.95 100.00% 40

5000-

n |-^ I'l , I l-i I I I 41 69 8487 6.40 6.60 6.80 7.00 5356 I 73 m/z 69.00 16.26% .................'"I m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63545:2-Pentanol, 4-methyl- 4b

MA i/?/7 I 5000- 6.40 6.60 6.80 7.00 69 "m/z 41705 12.41% 27 3942 , 57 w I' ......... m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63582: 2-Hexanol 40 6.40 6.60 6.80 7.00 5000 m/z 43.05 11.12%

27 69

m/z-> 19 I'''' I'''' I1^ 57 I ■ I" '-'1" " I 8487 TTTTtn+TTT 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1794: 2-Hexanol, (R)- ' ' 1 ' ' ' ' J ' ' ' ' I ‘ ' 1 ' ' ' ' I 4)5 6.40 6.60 6.80 7.00 m/z 4^/90 8.90% ft 5000

55 ? 8487 I" " I" " I' 1111 ■.. 11. ■' 11. ' ' I 'T* ' I ' I ' ' I ' ' ' ' I ' nZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00

22913.D NP091101.M Wed Oct 03 09:31:02 2001 Page 3

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