Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.
NYC-WTC_000087447–000087457Folder label: “GC/MS Scan 9/19/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
i Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\OCT0101\LBF.D Vial: 6 Acq On : 1 Oct 2001 6:37 pm Operator: 209 GALOS Sample : 9/19 Inst : GC/MS 209 Mise : *2x2- — bS/ Multiplr: 1.00 MS Integration Params: RTEINT.P , Oy/ Quant Time: Oct 1 19:25 2001 (^/nt Results File: NP091101.RES
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update : Thu Sep 13 12:47:04 2001 Response via : Initial Calibration DataAcq Meth ; NP091101
Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.79 152 524389 20.00 ug/1 -0.12 19) Naphthalene-d8 15.40 136 2030695 20.00 ug/1 -0.13 31) Acenaphthene-dlO 20.69. 164 959821 20.00 ug/1 -0.13 49) Phenanthrene-dlO 25.12 188 1383483 20.00 ug/1 -0.12 59) Chrysene-dl2 33.16 240 996051 20.00 ug/1 -0.12 68) Perylene-dl2 37.28 264 770421 20.00 ug/1 -0.14
System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = ... 0.00% 6) 2-Chlorophenol-d4 11.78 132 100 0.00 ug/1 0.37 Spiked Amount 75.000 Recovery = 0.00% 7) 1,2-Dichlorobenzene-d4 12.30 152 5571 0.22 ug/1 -0.13 Spiked Amount 50.000 Recovery = 0.44% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.83 172 2348 0.04 ug/1 0.02 Spiked Amount 50.000 Recovery = 0.08% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 0.00 244 0 0.00 ug/1 Spiked Amount -50.000 Recovery = 0.00%
Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis (2-CITTbroethyl) ether 0.00 93 0 N.TI.' • 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D. 17) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 N.D.
(#) = qualifier out of range (m) = manual integration LBF.D NP091101.M Wed Oct 03 14:31:33 2001 Page 1
NYC-WTC_000087447
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NYC-WTC_000088491
Calibration data table for TCLP analysis using GC/MS standards processed on October 18, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069732
Calibration table listing standard compounds and response values for GCMS analysis dated November 16, 2001.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067428
Laboratory report detailing GCMS analysis of sample AD22558 conducted on October 1, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068400
Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068559
Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067623
DEP lab report for GCMS analysis of sample AD23914 conducted on October 25, 2001, noting unknown compounds.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068230
Technical data sheet listing calibration standards and response factors for various polycyclic aromatic hydrocarbons.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069271
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 6, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068815
Calibration data sheet for GC/MS instrument listing standards like naphthalene-d8 used for testing on November 6, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067739
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 25, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069030
Calibration record for GC/MS instrument using TCLP method, listing standard compounds and response data from November 6, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.993
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