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GC/MS analysis results for sample AD22754, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22754 conducted on October 11, 2001, noting other unknown compounds.

NYC-WTC_000087403–000087416

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087415
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2801\22754.D Acq On : 29 Sep 2001 6:05 am Ope .’■■■9 GALOS Sample : gc/ms unknown tnr- EE 'MS 209 Mise : 3.00 MS Integration Params: LSCINT.P

Quant Method : C; \HPCHEM\1\METHODS\NPO91101 .M (RTE :!-tec or Title : 209 625/TCLP calibration table 7/16/71 Library : C:\DATABASE\NBS75K.L ***************************************************** ** * r V * * *

Peak Number 5 1,4-Dichlorobenzene-d4 Conceoti r a. 3

R.T. EstConc Area Relative to IST-i

11.65 0.52 ug/1 60696 1,4-Dichloroben2eYe- Hit# of 5 'entative ID MW MolForm Qual 1 1,4-Dj^3nlorobenzene-d4 150 C6C12r4 no :353-H3-l 53 2 Benz^l^e-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 oc;;i9a- 59-1 35 3 Benzaldehyde, 2-hydroxy-3-methoxy­ 152 C8H8O3 Of 314.'!-53-8 10 4 A<^naphthylene 152 C12H8 Of n;0:’-70-8 9 Abundance Scan 719(11.645 min): 22754.D (-) ‘ m/ . '•... EC !7oo% 1$0 i 5000 115 52 78 ■JO 40 I ®7 nrUUpr ”.'8 3 % TiZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 1!i0

5000 115 78 1' ? !,?.00_ 52 iii 3 .'■'77%

nfe-> 30 35 40 50 . ,..11,..?.. ,,,,1,1..... 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5.6-dichloro- 1!i0

115 11,40 : ;.ao ;:.oo 5000 52 78 m/ 7i3 I. 1 i. 74^

35 87 I I ' I' ' ' ' I ' mfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- i;i2 Z 106 53 81

122 ' ' I ' ' ' ' I ' ' ' ' I ' ' ' I' 92 ’T+’ 4UX I 136 ' I ' ' ' ' I ' ' ' ' I ■nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.40 _J

22754.D NP091101.M Fri Oct 05 15:21:43 2001 ace 5

NYC-WTC_000087415

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NYC-WTC_000087415Source: NYC Law Department, mirrored locally

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