Calibration data table for TCLP analysis including retention times and response factors for various compounds.
NYC-WTC_000086981–000087006Folder label: “508 Scan 9/17/01 9/26/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed) '■Data File : C:\HPCHEM\1\DATA\OCT0101\LBD.D Vial: 4 Acq On : 1 Oct 2001.4:39 pm Operator: 209 GALOS Sample : 9/17 Inst : GC/MS 209 Multiplr; 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 2 12:20 2001 Quant Results File; NP091101.RES Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update ; Thu Sep 13 12:47.: 04 2 001 /y a U f Response via : Initial Calibration / DataAcq Meth : NPO91101 /X / A
Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.79 152 517132 20.00 ug/1 -0.12 19) Naphthalene-d8 15.40 136 2016888 20.00 ug/1 -0.13 31) Acenaphthene-dlO 20.69 164 942725 20.00 ug/1 -0.13 49) Phenanthrene-dlO 25.12 188 1354803 20.00 ug/1 -0.12 59) Chrysene-dl2 33.16 240 1003514 20.00 ug/1 -0.12 68) Perylene-dl2 37.28 264 760704 20.00 ug/1 -0.14
System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 0.00 132 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 7) 1,2-Dichlorobenzene-d4 12.30 152 5377 0.21 ug/1 -0.13 Spiked Amount 50.000 Recovery = 0.42% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.83 172 2289 0.04 ug/1 0.02 Spiked Amount 50.000 Recovery = 0.08% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 30.00 244 198 0.00 ug/1 -0.15 Spiked Amount 50.000 Recovery = 0.00% Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D. 17) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 N.D.
(#) = qualifier out of range (m) = manual integration LBD.D NP091101.M Tue Oct 02 12:51:49 2001 Page 1
NYC-WTC_000086981
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GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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